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Quality Control Results <br />Job Number: 720-1310-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />01/06/2006 1348 <br />01/06/2006 1417 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3933 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />01/05/2006 1144 <br />Prep Batch: 720-3933 <br />Analysis Batch: 720-4061 <br />c:\saturnws\data\200601\010606 <br />30.48 g <br />1 mL <br />c:\saturnws\data\200601\010606\ <br />30.12 g <br />1 mL <br />mg/Kg <br />01/05/2006 1144 <br />Analysis Batch: 720-4061 <br />Prep Batch: 720-3933 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />LCS 720-3933/2-A <br />LCSD 720-3933/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />8374 5 - 112 13 35Phenol <br />8176 12 - 158 8 35Bis(2-chloroethyl)ether <br />7668 23 - 134 11 352-Chlorophenol <br />7868 9 - 172 15 351,3-Dichlorobenzene <br />8072 20 - 124 12 351,4-Dichlorobenzene <br />8676 10 - 130 14 35Benzyl alcohol <br />7770 32 - 129 11 351,2-Dichlorobenzene <br />8570 10 - 130 21 352-Methylphenol <br />142120 10 - 130 17 35 *4-Methylphenol <br />8676 9 - 230 12 35N-Nitrosodi-n-propylamine <br />8870 40 - 113 24 35Hexachloroethane <br />7987 35 - 180 8 35Nitrobenzene <br />9092 21 - 196 2 35Isophorone <br />8492 29 - 182 8 352-Nitrophenol <br />8188 32 - 119 7 352,4-Dimethylphenol <br />8988 33 - 184 2 35Bis(2-chloroethoxy)methane <br />9287 10 - 130 7 352,4-Dichlorophenol <br />8396 44 - 142 13 351,2,4-Trichlorobenzene <br />8384 21 - 133 0 35Naphthalene <br />3540 10 - 130 11 354-Chloroaniline <br />7380 24 - 116 8 35Hexachlorobutadiene <br />9187 10 - 130 5 354-Chloro-3-methylphenol <br />8285 10 - 130 3 352-Methylnaphthalene <br />8182 10 - 130 0 35Hexachlorocyclopentadiene <br />8180 37 - 144 3 352,4,6-Trichlorophenol <br />8476 10 - 130 11 352,4,5-Trichlorophenol <br />8381 10 - 130 4 352-Chloronaphthalene <br />8180 10 - 130 3 352-Nitroaniline <br />9395 9 - 112 1 35Dimethyl phthalate <br />8980 33 - 145 11 35Acenaphthylene <br />7769 10 - 130 13 353-Nitroaniline <br />8478 47 - 145 8 35Acenaphthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 159 of 186