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Quality Control Results <br />Job Number: 720-1310-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />01/06/2006 1348 <br />01/06/2006 1417 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3933 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />01/05/2006 1144 <br />Prep Batch: 720-3933 <br />Analysis Batch: 720-4061 <br />c:\saturnws\data\200601\010606 <br />30.48 g <br />1 mL <br />c:\saturnws\data\200601\010606\ <br />30.12 g <br />1 mL <br />mg/Kg <br />01/05/2006 1144 <br />Analysis Batch: 720-4061 <br />Prep Batch: 720-3933 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />LCS 720-3933/2-A <br />LCSD 720-3933/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />8780 9 - 191 10 352,4-Dinitrophenol <br />111104 10 - 130 8 354-Nitrophenol <br />7976 10 - 130 5 35Dibenzofuran <br />9288 39 - 139 6 352,4-Dinitrotoluene <br />9185 50 - 158 8 352,6-Dinitrotoluene <br />8686 9 - 114 1 35Diethyl phthalate <br />9076 25 - 158 18 354-Chlorophenyl phenyl ether <br />8481 59 - 121 5 35Fluorene <br />8587 10 - 130 2 354-Nitroaniline <br />9597 9 - 181 1 352-Methyl-4,6-dinitrophenol <br />98102 10 - 130 3 35N-Nitrosodiphenylamine <br />8688 53 - 127 1 354-Bromophenyl phenyl ether <br />8478 9 - 152 9 35Hexachlorobenzene <br />9593 14 - 176 3 35Pentachlorophenol <br />9289 10 - 130 5 35Phenanthrene <br />8789 27 - 133 1 35Anthracene <br />9194 10 - 130 3 35Di-n-butyl phthalate <br />91101 26 - 137 9 35Fluoranthene <br />8582 52 - 115 5 35Pyrene <br />9087 10 - 130 5 35Butyl benzyl phthalate <br />6874 10 - 130 8 353,3'-Dichlorobenzidine <br />8786 33 - 143 2 35Benzo[a]anthracene <br />9287 8 - 158 7 35Bis(2-ethylhexyl) phthalate <br />8086 17 - 168 6 35Chrysene <br />8581 4 - 146 6 35Di-n-octyl phthalate <br />8990 24 - 159 1 35Benzo[b]fluoranthene <br />8993 17 - 163 3 35Benzo[a]pyrene <br />8483 11 - 162 2 35Benzo[k]fluoranthene <br />091 9 - 171 200 35 *Indeno[1,2,3-cd]pyrene <br />8792 9 - 219 4 35Benzo[g,h,i]perylene <br />3837 10 - 130 4 35Benzoic acid <br />8480 10 - 130 6 35Azobenzene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 160 of 186