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Quality Control Results <br />Job Number: 720-1310-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />01/06/2006 1935 <br />01/06/2006 2004 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3933 <br />5.0 <br />5.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-4061 <br />Analysis Batch: 720-4061 <br />01/05/2006 1144 <br />01/05/2006 1144 <br />Prep Batch: 720-3933 <br />Prep Batch: 720-3933 <br />c:\saturnws\data\200601\010 <br />30.45 g <br />5 mL <br />c:\saturnws\data\200601\0106 <br />30.39 g <br />5 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />720-1310-1 <br />720-1310-1 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />64 59 5 - 112 8 35Phenol <br />55 52 12 - 158 5 35Bis(2-chloroethyl)ether <br />69 73 23 - 134 6 352-Chlorophenol <br />60 58 9 - 172 2 351,3-Dichlorobenzene <br />61 58 20 - 124 4 351,4-Dichlorobenzene <br />51 34 10 - 130 42 35 *Benzyl alcohol <br />63 68 32 - 129 9 351,2-Dichlorobenzene <br />84 85 10 - 130 2 352-Methylphenol <br />146 160 10 - 130 9 35 **4-Methylphenol <br />66 92 9 - 230 NC 35N-Nitrosodi-n-propylamine <br />69 89 40 - 113 25 35Hexachloroethane <br />59 61 35 - 180 2 35Nitrobenzene <br />89 87 21 - 196 2 35Isophorone <br />65 83 29 - 182 23 352-Nitrophenol <br />79 85 32 - 119 8 352,4-Dimethylphenol <br />77 81 33 - 184 4 35Bis(2-chloroethoxy)methane <br />79 94 10 - 130 17 352,4-Dichlorophenol <br />87 87 44 - 142 0 351,2,4-Trichlorobenzene <br />85 92 21 - 133 8 35Naphthalene <br />21 18 10 - 130 NC 354-Chloroaniline <br />78 88 24 - 116 13 35Hexachlorobutadiene <br />70 73 10 - 130 5 354-Chloro-3-methylphenol <br />91 95 10 - 130 5 352-Methylnaphthalene <br />45 34 10 - 130 28 35Hexachlorocyclopentadiene <br />81 79 37 - 144 2 352,4,6-Trichlorophenol <br />79 74 10 - 130 6 352,4,5-Trichlorophenol <br />97 90 10 - 130 7 352-Chloronaphthalene <br />87 87 10 - 130 0 352-Nitroaniline <br />102 104 9 - 112 2 35Dimethyl phthalate <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 162 of 186