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Quality Control Results <br />Job Number: 720-1310-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />01/06/2006 1935 <br />01/06/2006 2004 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3933 <br />5.0 <br />5.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-4061 <br />Analysis Batch: 720-4061 <br />01/05/2006 1144 <br />01/05/2006 1144 <br />Prep Batch: 720-3933 <br />Prep Batch: 720-3933 <br />c:\saturnws\data\200601\010 <br />30.45 g <br />5 mL <br />c:\saturnws\data\200601\0106 <br />30.39 g <br />5 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />720-1310-1 <br />720-1310-1 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />97 102 33 - 145 5 35Acenaphthylene <br />33 83 10 - 130 86 35 *3-Nitroaniline <br />97 103 47 - 145 6 35Acenaphthene <br />333 320 9 - 191 4 35 **2,4-Dinitrophenol <br />83 81 10 - 130 3 354-Nitrophenol <br />87 91 10 - 130 4 35Dibenzofuran <br />91 101 39 - 139 11 352,4-Dinitrotoluene <br />98 114 50 - 158 16 352,6-Dinitrotoluene <br />104 118 9 - 114 12 35 *Diethyl phthalate <br />101 95 25 - 158 6 354-Chlorophenyl phenyl ether <br />95 96 59 - 121 2 35Fluorene <br />90 79 10 - 130 13 354-Nitroaniline <br />48 23 9 - 181 NC 352-Methyl-4,6-dinitrophenol <br />100 99 10 - 130 1 35N-Nitrosodiphenylamine <br />89 97 53 - 127 8 354-Bromophenyl phenyl ether <br />96 87 9 - 152 10 35Hexachlorobenzene <br />69 68 14 - 176 1 35Pentachlorophenol <br />104 105 10 - 130 1 35Phenanthrene <br />100 103 27 - 133 3 35Anthracene <br />105 116 10 - 130 10 35Di-n-butyl phthalate <br />101 123 26 - 137 20 35Fluoranthene <br />102 94 52 - 115 8 35Pyrene <br />96 101 10 - 130 6 35Butyl benzyl phthalate <br />56 68 10 - 130 20 353,3'-Dichlorobenzidine <br />88 63 33 - 143 34 35Benzo[a]anthracene <br />98 102 8 - 158 4 35Bis(2-ethylhexyl) phthalate <br />96 78 17 - 168 20 35Chrysene <br />67 70 4 - 146 3 35Di-n-octyl phthalate <br />110 110 24 - 159 0 35Benzo[b]fluoranthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 163 of 186