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Quality Control Results <br />Job Number: 720-1310-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />01/06/2006 1935 <br />01/06/2006 2004 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3933 <br />5.0 <br />5.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-4061 <br />Analysis Batch: 720-4061 <br />01/05/2006 1144 <br />01/05/2006 1144 <br />Prep Batch: 720-3933 <br />Prep Batch: 720-3933 <br />c:\saturnws\data\200601\010 <br />30.45 g <br />5 mL <br />c:\saturnws\data\200601\0106 <br />30.39 g <br />5 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />720-1310-1 <br />720-1310-1 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />101 98 17 - 163 2 35Benzo[a]pyrene <br />91 95 11 - 162 5 35Benzo[k]fluoranthene <br />96 109 9 - 171 13 35Indeno[1,2,3-cd]pyrene <br />97 100 9 - 219 3 35Benzo[g,h,i]perylene <br />0 0 10 - 130 NC 35 **Benzoic acid <br />86 87 10 - 130 1 35Azobenzene <br />86 85 10 - 130 NC 35Dibenz(a,h)anthracene <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />Nitrobenzene-d5 55 49 23 - 120 <br />2-Fluorobiphenyl 94 80 30 - 115 <br />Terphenyl-d14 94 90 18 - 137 <br />2-Fluorophenol 49 58 25 - 121 <br />Phenol-d5 63 57 24 - 113 <br />2,4,6-Tribromophenol 96 99 19 - 122 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 164 of 186