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Quality Control Results <br />Job Number: 720-993-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/19/2005 1852 <br />12/19/2005 1922 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3184 <br />5.0 <br />5.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3246 <br />Analysis Batch: 720-3246 <br />12/16/2005 1549 <br />12/16/2005 1549 <br />Prep Batch: 720-3184 <br />Prep Batch: 720-3184 <br />d:\data\200512\121905\720-9 <br />30.36 g <br />1 mL <br />d:\data\200512\121905\720-99 <br />30.48 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-993-10 <br />720-993-10 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />58 42 5 - 112 30 35Phenol <br />48 38 12 - 158 24 35Bis(2-chloroethyl)ether <br />46 37 23 - 134 22 352-Chlorophenol <br />45 42 9 - 172 8 351,3-Dichlorobenzene <br />47 41 20 - 124 12 351,4-Dichlorobenzene <br />41 30 10 - 130 32 35Benzyl alcohol <br />49 42 32 - 129 15 351,2-Dichlorobenzene <br />44 33 10 - 130 30 352-Methylphenol <br />91 64 10 - 130 36 35 *4-Methylphenol <br />44 31 9 - 230 36 35 *N-Nitrosodi-n-propylamine <br />47 42 40 - 113 11 35Hexachloroethane <br />56 45 35 - 180 23 35Nitrobenzene <br />59 40 21 - 196 40 35 *Isophorone <br />50 42 29 - 182 18 352-Nitrophenol <br />33 24 32 - 119 33 35 *2,4-Dimethylphenol <br />52 38 33 - 184 31 35Bis(2-chloroethoxy)methane <br />56 40 10 - 130 34 352,4-Dichlorophenol <br />50 39 44 - 142 24 35 *1,2,4-Trichlorobenzene <br />52 45 21 - 133 14 35Naphthalene <br />24 18 10 - 130 32 354-Chloroaniline <br />58 44 24 - 116 28 35Hexachlorobutadiene <br />59 43 10 - 130 33 354-Chloro-3-methylphenol <br />57 48 10 - 130 19 352-Methylnaphthalene <br />48 32 10 - 130 41 35 *Hexachlorocyclopentadiene <br />61 42 37 - 144 36 35 *2,4,6-Trichlorophenol <br />76 45 10 - 130 50 35 *2,4,5-Trichlorophenol <br />64 50 10 - 130 25 352-Chloronaphthalene <br />67 46 10 - 130 37 35 *2-Nitroaniline <br />69 42 9 - 112 48 35 *Dimethyl phthalate <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 119 of 141