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Quality Control Results <br />Job Number: 720-993-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/19/2005 1852 <br />12/19/2005 1922 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3184 <br />5.0 <br />5.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3246 <br />Analysis Batch: 720-3246 <br />12/16/2005 1549 <br />12/16/2005 1549 <br />Prep Batch: 720-3184 <br />Prep Batch: 720-3184 <br />d:\data\200512\121905\720-9 <br />30.36 g <br />1 mL <br />d:\data\200512\121905\720-99 <br />30.48 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-993-10 <br />720-993-10 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />85 59 33 - 145 37 35 *Acenaphthylene <br />71 46 10 - 130 44 35 *3-Nitroaniline <br />70 49 47 - 145 35 35Acenaphthene <br />11 4 9 - 191 NC 35 *2,4-Dinitrophenol <br />74 53 10 - 130 34 354-Nitrophenol <br />73 50 10 - 130 37 35 *Dibenzofuran <br />66 44 39 - 139 40 35 *2,4-Dinitrotoluene <br />83 55 50 - 158 42 35 *2,6-Dinitrotoluene <br />84 58 9 - 114 37 35 *Diethyl phthalate <br />80 54 25 - 158 38 35 *4-Chlorophenyl phenyl ether <br />78 52 59 - 121 41 35 *Fluorene <br />73 46 10 - 130 45 35 *4-Nitroaniline <br />28 12 9 - 181 NC 352-Methyl-4,6-dinitrophenol <br />74 49 10 - 130 41 35 *N-Nitrosodiphenylamine <br />53 34 53 - 127 44 35 *4-Bromophenyl phenyl ether <br />77 52 9 - 152 40 35 *Hexachlorobenzene <br />45 27 14 - 176 50 35 *Pentachlorophenol <br />84 50 10 - 130 52 35 *Phenanthrene <br />75 46 27 - 133 48 35 *Anthracene <br />93 56 10 - 130 50 35 *Di-n-butyl phthalate <br />86 52 26 - 137 50 35 *Fluoranthene <br />87 53 52 - 115 49 35 *Pyrene <br />90 58 10 - 130 44 35 *Butyl benzyl phthalate <br />26 18 10 - 130 37 35 *3,3'-Dichlorobenzidine <br />48 32 33 - 143 39 35 *Benzo[a]anthracene <br />87 51 8 - 158 53 35 *Bis(2-ethylhexyl) phthalate <br />93 56 17 - 168 50 35 *Chrysene <br />86 47 4 - 146 58 35 *Di-n-octyl phthalate <br />74 49 24 - 159 41 35 *Benzo[b]fluoranthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 120 of 141