Laserfiche WebLink
Quality Control Results <br />Job Number: 720-993-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/19/2005 1852 <br />12/19/2005 1922 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3184 <br />5.0 <br />5.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3246 <br />Analysis Batch: 720-3246 <br />12/16/2005 1549 <br />12/16/2005 1549 <br />Prep Batch: 720-3184 <br />Prep Batch: 720-3184 <br />d:\data\200512\121905\720-9 <br />30.36 g <br />1 mL <br />d:\data\200512\121905\720-99 <br />30.48 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-993-10 <br />720-993-10 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />73 48 17 - 163 43 35 *Benzo[a]pyrene <br />69 44 11 - 162 44 35 *Benzo[k]fluoranthene <br />70 44 9 - 171 46 35 *Indeno[1,2,3-cd]pyrene <br />79 50 9 - 219 45 35 *Benzo[g,h,i]perylene <br />1 0 10 - 130 NC 35 **Benzoic acid <br />74 45 10 - 130 49 35 *Azobenzene <br />73 47 10 - 130 NC 35Dibenz(a,h)anthracene <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />Nitrobenzene-d5 53 42 23 - 120 <br />2-Fluorobiphenyl 69 54 30 - 115 <br />Terphenyl-d14 81 50 18 - 137 <br />2-Fluorophenol 45 38 25 - 121 <br />Phenol-d5 50 38 24 - 113 <br />2,4,6-Tribromophenol 69 50 19 - 122 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 121 of 141