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March 27, 2020 Lab ID : STK2O32768 Frank C Alegre Trucking Inc. Customer : 3-13002 Quality Control-Inorganic Constituent Method Date/ID Type Units Conc. QC Data DQO Note Metals Barium 6010B 03/10/20:203864AC CCB ppm -0.0003 0.03 CCV ppm 1.000 104% 90-110 CCB ppm -0.0002 0.03 Beryllium 6010B 03/05/20:203811AC CCV ppm 1.000 96.3% 90-110 CCB ppm -0.00009 0.005 CCV ppm 1.000 -0.01% 90-110 CCB ppm -0.00011 1 0.005 Cadmium 6010B 03/10/20:203864AC CCV ppm 1.000 100% 90-110 CCB ppm 0.00008 0.005 CCV ppm 1.000 99.4% 90-110 CCB ppm -0.0001 0.005 Chromium 6010B 03/05/20:203811AC CCV ppm 1.000 96.4% 90-110 CCB ppm 0.0011 0.01 CCV ppm 1.000 0.2% 90-110 CCB ppm 1 0.0016 0.01 Cobalt 6010B 03/05/20:203811AC CCV ppm 1.000 95.4% 90-110 CCB ppm -0.0005 0.01 CCV ppm 1.000 -0.06% 90-110 CCB ppm 0.0002 0.01 6010B 03/14/20:204056AC CCV ppm 1.000 94.5% 90-110 CCB ppm -0.00005 0.01 CCV ppm 1.000 93.6% 90-110 CCB ppm 0.0010 1 0.01 Copper 6010B 03/05/20:203811AC CCV ppm 1.000 95.2% 90-110 CCB ppm 0.0154 0.01 220 CCV ppm 1.000 1.5% 90-110 CCB p m 0.0139 0.01 220 6010B 03/10/20:203864AC CCV ppm 1.000 102% 90-110 CCB ppm 0.0015 0.01 CCV ppm 1.000 102% 90-110 CCB ppm 0.0021 1 0.01 Lead 6010B 03/05/20:203811AC CCV ppm 1.000 102% 90-110 CCB ppm -0.0020 0.01 CCV ppm 1.000 -0.09% 90-110 CCB ppm -0.0022 0.01 Molybdenum 6010B 03/10/20:203864AC CCV ppm 1.000 100% 90-110 CCB ppm -0.0085 0.01 CCV ppm 1.000 100% 90-110 CCB ppm 1 -0.0025 0.01 Nickel 6010B 03/05/20:203811AC CCV ppm 1.000 96.7% 90-110 CCB ppm -0.0007 0.01 CCV ppm 1.000 -0.09% 90-110 CCB p m -0.0012 0.01 Selenium 6010B 03/12/20:203859AC CCV ppm 1.000 107% 90-110 CCB ppm 0.0017 0.02 CCV ppm 1.000 107% 90-110 CCB ppm 0.0004 1 0.02 Silver 6010B 03/10/20:203864AC CCV ppm 1.000 97.2% 90-110 CCB ppm -0.0009 0.02 CCV ppm 1.000 96.6% 90-110 CCB ppm -0.0005 0.02 Thallium 6010B 03/05/20:203811AC CCV ppm 1.000 98.0% 90-110 CCB ppm -0.0021 0.02 CCV ppm 1 1.000 1 -0.2% 1 90-110 Page 7 of 8