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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> )t=//www mccamnbel l cQM E-mail main@mccampbell corn <br /> Date Sampled 12/04/98 <br /> Advanced GeoEnvironmental Client Project ID Newfield Property <br /> 4005 North Wilson Way <br /> Date Received 12/05/98 <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 12/08/98 <br /> Client P O Date Analyzed 12/08/98 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 99689 <br /> Client ID MW-1-12-4-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<35 Ethylbenzene 23 <br /> Benzene 37 Hexachlorobutadiene ND<5 <br /> Bromobenzene ND<5 lodomethane ND<5 <br /> Bromochloromethane ND<5 lsopropyibenzene ND<5 <br /> Bromodichloromethane ND<5 p-Isopropyl toluene ND<5 <br /> Bromoform ND<5 Methyl butyl ketoneND<5 <br /> Bromomethane ND<5 Methylene Chlonde"' ND<25 <br /> n-Butyl benzene ND<5 Methyl ethyl ketone' ND<5 <br /> sec-Butyl benzene ND<5 Methyl isobutyl ketone & ND<5 <br /> teri-Butyl benzene ND<5 Methyl tent-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<5 Napthalene ND<5 <br /> Carbon Tetrachloride ND<5 n-Propyl benzene 56 <br /> Chlorobenzene ND<5 Styrene' ND<5 <br /> Ii Chloroethane ND<5 1,1,1,2-Tetrachloroethane N EK5 <br /> 2-Chloroethyl Vinyl Ether") ND<5 1,1,2,2-Tetrachloroethane ND<5 <br /> Chloroform 16 Tetrachloroethene ND<20 <br /> Chloromethane ND<5 Toluene` 240 <br /> 2-Chlorotoluene ND<5 1,2,3-Tnchl orobenzene ND<5 <br /> 4-Chlorotoluene ND<5 I,2,4-Tnchl orobenzen e ND<5 <br /> Di bromochloromethan e ND<5 1,1,1-Trichloroethane ND�5 <br /> 1 2 Dibromo-3-chloropropane ND<5 1,1,2-Tnchloroethane ND<5 <br /> Dibromomethane ND<5 Trichloroethene ND<5 <br /> 1,2-Dichlorobenzene ND<5 Tnchiorofluoromethane ND<5 <br /> I 1,3 Dichlorobenzene NEX5 1,2,3-Tnchloropropane ND<5 <br /> 1,4 Dichlorobenzene ND<5 1,2,4-Trimethylbenzene 34 <br /> Dichlorodifluoromethane ND<5 1,3,5-Trimethylbenzen e 13 <br /> 1,]-Dichloroethane ND<5 Vinyl Acetate"I ND<5 <br /> 1,2 Dichloroethane 15 Vinyl Chloride ") ND<5 <br /> 1,1-Dichloroethene ND<5 Xylenes,total '° 160 <br /> cis-l,2-Dichtoroethene ND<5 <br /> trans-1,2-Dichloroethene ND<5 <br /> 1,2-Dichloropropane ND<5 <br /> l,3-Dich]oropropane ND<5 <br /> 2,2-Dichloropropane ND<5 Comments i <br /> 1,1-Dichioropropene ND<5 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<5 Dibromofluoromethane 104 <br /> trans-1,3-Dichloropropene ND<5 Toluene-d8 85 <br /> - thylene dibromide ND<5 4-Bromofluorobenzene 102 <br /> "ate,and vapor samples are reported m ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> I sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattem of our standard for <br /> this analyte (1)methylbenzene,(m)acenc acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 //^ Edward Hamilton,Lab Director <br />