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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> y EUp//www mccampbell com E-mail main@mccampbell com <br />` Date Sampled 12/04/98 <br /> li Advanced GeoEnvironmental Client Project ID Newfield Property <br /> D <br /> 4005 North Wilson Way ate Received 12/05/98 <br /> F Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 12/08/98 <br /> I Client P O Date Analyzed 12/08/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 99690 <br /> Client ID MW-2-12-4-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<650 Ethylbenzene 1100 <br /> Benzene 4500 Hexachlorobutadiene ND<130 <br /> Bromobenzene ND<130 Iodomethane ND<130 <br /> Bromochloromethane ND<130 Isopropylbenzene ND<130 <br /> Bromodichloromethane ND<130 p-Isopropyl toluene ND<130 <br /> IBromoform ND<130 Methyl butyl ketone ' ND<130 <br /> Bromomethane ND<130 Methylene Chloride"' ND<130 <br /> n-Butyl benzene ND<l30 Methyl ethyl ketoneND<130 <br /> sec-Butyl benzene ND<l30 Methyl isobutyl ketone`6 ND<130 <br /> tert-Butyl benzene ND<130 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<130 Napthalene ND<130 <br /> Carbon Tetrachloride ND<130 n-Propyl benzene 160 <br /> Chlorobenzene ND<130 Styrene' ND<130 <br /> Chloroethane ND<130 1,1,1,2 Tetrachloroethane ND<130 <br /> 2-Chloroethyl Vinyl Ether" ND<130 1,1,2,2 Tetrachloroethane ND<130 <br /> Chloroform ND<130 Tetrachloroethene ND<t 30 <br /> Chloromethane ND<130 Toluene ' 4200 <br /> 2-Chlorotoluene N D<130 1,2,3-Tri chl orobenzen a ND<130 <br /> 4-Chlorotoluene ND<130 1,2,4-Tn chlorobenzene NIXI 30 <br /> Dibromochloromethane ND<130 1,1,1-Tnchloroethanc ND<130 <br /> 1,2-Dibromo-3-chloropropane ND<130 11,2-Tnchloroethane ND<130 <br /> Dibromomethane ND<130 Trichloroethene ND<130 <br /> 1,2 Dichlorobenzene ND<130 Tnehlorofluoromethane ND<130 <br /> 1,3-Dichlorobenzene N13<130 1,2,3-Tn chloropropane ND<130 <br /> 1,4-Dichlorobenzene ND<130 1,2,4-Tn methylbenzene 1100 <br /> DichlOrodlfluoromelhanL ND<130 1,3,5-Tnmethylbenzene 260 <br /> 1,1-Dichloroethane ND<130 Vinyl Acetate"" ND<130 <br /> 1,2-Dichloroethane 540 Vinyl Chloride ND<130 <br /> 1,1-Dichloroethene ND<130 Xylenes,total `° 5100 <br /> cis-1,2-Dichloroethene ND<130 <br /> tr2ns-1,2-Dichloroethene ND<130 <br /> 1,2-Dichloropropane ND<130 <br /> 1,3-Dichloropropane ND<130 <br /> 2 2-Dichloropropane ND<130 Comments <br /> 1,1-Dichloropropene ND<130 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<110 Dibromofluoromethane 105 <br /> trans-l,3-Dichloropropene ND<130 Toluene-d8 86 <br /> Ethylene dibromide ND<130 4-Bromofluorobenzene 110 <br /> >,,ater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipc and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(I)methylbenzene,(m)acetic acrd ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 //1 Edward Hamilton, Lab Director <br />