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Q 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ® McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> //www mccamnbell coin E-mail main@mecampbell eom <br /> Date Sampled 12/04/98 <br /> Advanced GeoEnvironmental Client Protect ID Newfield Property <br /> 4005 North Wilson Way <br /> Date Received 12/05/98 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 12/08/98 <br /> Client P O Date Analyzed 12/08/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 99692 <br /> Client ID MW-4-12-4-98 <br /> Matrix W <br /> 4 <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<150 Ethylbenzene 46 <br /> Benzene 30 Hexachlorobutadiene ND<10 <br /> Bromobenzene ND<10 lodomethane ND<10 <br /> Bromochioromethane ND<10 lsopropylbenzene 22 <br /> B70mOdiehloTomethane ND<10 p-Isopropyl toluene ND<l0 <br /> Bromoform ND<10 Methyl butyl ketone ND<10 <br /> Bromomethane ND<10 Methylene Chlonde" ND<10 <br /> n-Butyl benzene 18 Methyl ethyl ketone` ND<10 <br /> sec-Butyl benzene ND<10 Methyl tsobutyl ketone`8 ND<10 <br /> F tert-Butyl benzene ND<10 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<10 Napthalene ND<30 <br /> Carbon Tetrachloride ND<10 n-Propyl benzene 197 <br /> Chlorobenzene ND<10 Styrene ND<10 <br /> 4 Ch1 orocthane ND<10 1,1,1,2-Tetrachloroethane ND<10 <br /> 2-Chloroethyl Vinyl Ether ND<10 1,1,2,2-Tetrachloroethane ND<10 <br /> Chloroform ND<10 Tetrachloroethene ND<10 <br /> C Chloromethane ND<10 Toluene"J 300 <br /> 2-Ch I oratoluene ND<10 1,2,3-Tnchlorobenzene ND<10 <br /> 4-Chlorotoluene ND<10 1,2,4-Tnchlorobenzene ND<10 <br /> Dibromochloromethane ND<10 1,1,1 Tnchloroethane ND<]0 <br /> C1,2-Dibromo-3-chioropropane ND<10 1,1,2-Tnchloroethane ND<10 <br /> IDibromomethane ND<10 Tnchloroethane ND<10 <br /> 1,2-Dichlorobenzene ND<10 Tnchlorofluoromethane ND<10 <br /> 1,3-Dichlorobenzene ND<10 1,2,3-Tnehloropropane ND<]0 <br />` 1,4-Dichlorobenzene ND<10 1,2,4-Tnmethylbenzene 75 <br /> IDichlorodifluoromethane ND<10 1,3,5-Tnmethyl benzene 28 <br /> 1,1-Dichloroethane ND<10 Vinyl Acetate"1 27 <br /> 1,2-Dichloroethane 370 Vinyl Chloride`" ND<10 <br /> 1,1-Dichloroethene ND<10 Xylenes,total 87 <br /> cis-1,2-Dichloroethene ND<10 <br /> Iran s-],2-Dichloroethene ND<10 <br /> 1,2-Dichloropropane ND<10 <br /> 1,3-Dichloropropane ND<10 <br /> 2,2-Dichloropropane ND<10 Comments <br /> 1,1-Dichloropropene ND<10 Surrogate RecoNeries(%) <br /> cis-1,3-Dtchloropropene ND<10 Dibromofluoromethane <br /> trans-1,3-Dichloropropene ND<10 Toluene-d8 <br /> Ethylene dibromide ND<10 4-Bromofluorobenzene <br /> kater and vapor samples are reported m ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated Hater samples 1 0 ug/L, vapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected abo%a the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-cbloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peals present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethane,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> f <br />