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I <br /> l I 10 Second Avenue South,#ID7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> k24 hJW//www.mccamgbell cam E-mail main@mccampbell com <br /> i <br /> Date Sampled 12/04/98 <br /> Advanced GeoEnvironmental Client Protect ID Newfield Property <br /> 4005 North Wilson Way <br /> Date Received 12/05/98 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 12/08/98 <br /> Client P O Date Analyzed 12/08/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8250 <br /> Lab 1D 99693 <br /> Client ID MW-5/12-4-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ' ND<8 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Brotnobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzene ND <br /> I Bromodichloromethane ND p lsopropyl toluene ND <br /> Bromoform ND Methyl butyl ketoneND <br /> Bromomethane ND Methylene Chlonde"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone` ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'8 ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND St}Tene' ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl£they" ND 1,1,2,2 Tetrachloroethane ND <br /> Chloroform ND Temchloroethene ND <br /> C Chioromethane ND Toluene 23 <br /> 2-Chlorotoluene ND 1,2 3-Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Tnch1orobenzene ND <br /> Dibromochlommethane ND 1,1,E-Tnchloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Tnchloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Tnchlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Tn chi oropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate"' ND <br /> 1,2-Dichloroethane ND Vinyl Chlonde"' ND <br /> I,1-Dichloroethene ND Xyicnes,total `° ND <br /> cis-1,2 Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 103 <br /> trans-l,3-Dichloropropene ND Toluene-d8 86 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 105 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected abox a the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimeth}] ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 r Edward Hamilton, Lab Director <br />