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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ehttp//www mccampbell corn E-mail main@mccampbell com <br /> Date Sampled 01l13-01115199 <br /> Advanced GeoEnvirownental Client Project ID Newfield Property <br /> Date Received 01/18/99 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 01/20/99 <br /> Client P O Date Analyzed 01/20/99 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 01889 <br /> Client ID B4/1-13-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ND<900 Ethylbenzene 1400 <br /> Benzene 2700 Hexachiorobutadiene ND<250 <br /> Bromobenzene ND<250 lodomethane ND<250 <br /> Bromochloromcthane ND<250 lsopropylbenzene ND<250 <br /> Bromodichloromethane ND<250 p-Isopropyl toluene ND<250 <br /> Bromoform ND<250 Methyl butyl ketone ND<250 <br /> Bromomethane ND<250 Methylene Chloride"' ND<250 <br /> n-Butyl benzene ND<250 Mcthyl ethyl ketone ' ND<250 <br /> sec-Butyl benzene ND<250 Meihyl isobutyl ketone`9 ND<250 <br /> ttrt-Butyl benzene ND<250 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<250 Napthalene ND<250 <br /> Carbon Tetrachloride ND<250 n-Propyl benzene 320 <br /> Chlorobenzene ND<250 Styrene ND<250 <br /> Chloroethane ND<250 1,1,1,2-Tetrachloroethane ND<250 <br /> 2 Chloroethyl Vinyl Ether"' ND<250 1,1 2,2-Tetrachloroethane ND<250 <br /> Chloroform ND<250 Tetrachloroethene ND<250 <br />' Chloromethane ND<250 Toluene N13<250 <br /> 2-Chlorotoluene ND<250 1,2,3-Tn chlorobenzene ND<250 <br /> 4 Chlarotolueiie ND<250 1,2,4-Tnchlorobenzene ND<250 <br /> Dibromochloromeihan e ND<250 1,1 1-Trichloroethane ND<250 <br /> 1,2-Dibromo-3-chloropropane ND<250 1,1,2-Tnchloroethane ND<250 <br /> Dibromomethane ND<250 Trichloroethene ND<250 <br /> 1,2-Dichlorobenzene ND<250 Trichlorofluoromethane ND<250 <br /> 1,3-Dichlorobenzene ND<250 1,2,3-Tnchloropropane ND<250 <br /> 1,4-Dichlorobenzene ND<250 1,2,4-Trimethylbenzene $20 <br /> Dichlorodifluoromethara, ND<250 1,3,5-Tnrnethylbenzene 250 <br /> 1,1-Dichloroethane ND<250 Vinyl Acetate" ND<250 <br />' 1 2-Dichloroethane ND<250 Vinyl Chloride ND<250 <br /> 1,1-Dichloroethene ND<250 Xylenes,total ° 3600 <br /> cis-1,2-Dichloroethene ND<250 <br /> trans-1,2-Dichloroethene ND<250 <br /> 1,2-Dichloropropane ND<250 <br /> 1 3-Dichloropropane ND<250 <br /> 2,2-Dichloropropane ND<250 Comments h,i <br /> 1 1-Dichloropropane ND<250 Surrogate Recotieries(%) <br />' cis-1,3-Dichloropropene ND<250 Dibromofluoromethane 99 <br /> trans-1,3-Dichloropropene ND<250 Toluene-d8 iO4 <br /> Ethylene dibromide ND<250 4-Bromofluorobenzene 108 <br /> nater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h) lighter than water immiscible sheen is present, (i)liquid 5arnple that contains greater than —5 vol % <br />' sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />