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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htM://www mccamnbell corn E-mail main@mccampbell com <br /> i <br /> Date Sampled 01113-01115199 <br /> Advanced GeoEnvironmental Client Project ID Newfield Property <br /> D <br /> 4005 North Wilson Way ate Received 01/18/99 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 01/20/99 <br /> Client P O Date Analyzed 01/20/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 01890 <br /> Client 1D B5/1-13-99 <br /> Matnx W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<2 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chlonde" ND<2 <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone ' ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> I • Chlorobenzene ND St)7ene I') ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1 1,2,2-Tetrachloroethane ND <br /> Chloroform ND Teirachloroethene ND<2 <br /> Chloromethane ND Toluene` ND <br /> 2-Chlorotoluene ND 1,2,3-Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND <br /> Dlbromochloromethane ND 1,11-Trichloroethane ND <br /> 1,2-Dtbromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND l 2 3-Trichtoropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 13,5-Trimethylbenzene ND <br /> 11-Dichloroethane ND Vin)IAcetate"I ND <br /> 1,2-Dichloroethane ND Vinyl Chloride " ND <br /> 1,1-Dichloroethene ND Xylenes,total ° ND <br /> cis-1,2-Dichloroethene ND <br /> trans-l,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments i <br /> 1,1-Dichloropropene ND Surrogate Reco%eries(%) <br /> I cis-1,3-Dichloropropene ND Dibromofluoromethane 100 <br /> trans-1,3-Dichloropropene ND Toluene-d8 104 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 90 <br /> I water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and 211 TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 05 ug/L, solid and sludge samples 5 uglkg, wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> . (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacelone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />