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110 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> bJW l/www mccampbell co m E-mail main@mccampbell com <br /> Date Sampled 01/13-01115/99 <br /> Advanced GeoEnvironmental Client Project ID Newfield Property <br /> Date Received 01/1$199 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 01/20/99 <br /> Client P O Date Analyzed 01/20/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 01891 <br />' Client 1D B6/1-14-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone" ND<25 Eth)lbenzene 54 <br /> Benzene 13 Hexachlorobutadiene ND<3 <br /> Bromobenzene ND<3 Iodomethane ND<3 <br /> Bromochloromethane ND<3 l sopropylbenzene 100 <br />' Bromodichloromethane ND<3 p-Isopropyl toluene 10 <br /> Bromoform ND<3 Methyl butyl ketone` ND<3 <br /> Bromomethane ND<3 Methylene Chloride" ND<3 <br /> n-Butyl benzene 40 Mcihyl ethyl ketone' ND<3 <br />' sec-Butyl benzene 27 N1 ethyl isobutyl ketone 18 ND<3 <br /> tent-Butyl benzene 3 7 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<3 Napihalene N13<3 <br /> Carbon Tetrachloride ND<3 n Propyl benzene 55 <br />'• Chlorobenzene ND<3 Styrene` ND<3 <br /> Chloroethane ND<3 1,1,1,2-Tetrachloroethane ND<3 <br /> 2-Chloroethyl Vinyl Ether" ND<3 3,1,2 2-Tetrachloroethane ND<3 <br /> Chloroform ND<3 Tetrachloroethene ND<5 <br />' Chloromethane N'D<3 Toluene ND<3 <br /> 2-Chlorotoluene ND<3 €,2,3-Tnchlorobenzene ND-3 <br /> 4-Chlorotoluene ND<3 1,2 4-Tnchlorobenzene ND<3 <br /> Dibromochioromethane ND<3 1,1,1-Trichloroethane ND<3 <br />' 1,2-Dibromo-3-chloropropane 1\D<3 11,2-Trichloroethane ND<3 <br /> Dibromomethane ND<3 Trichloroethene 6 2 <br /> 1,2-Dichlorobenzene ND<3 Trichlorofluoromethane ND<3 <br />' 1,3-Dichlorobenzene N13<3 1,2,3-Tnchloropropane ND<3 <br /> 1,4-Dichlorobenzene ND<3 1 2 4-Trimethylbenzene ND<3 <br /> Dichlorodifluoromethane ND<3 1,3,5-Tnmethylbenzene ND<3 <br /> 1,1-Dichloroethane ND<3 Vin)l Acetate"1 67 <br /> 1,2-Dichloroethane 18 Vinyl Chloride " ND<3 <br /> 1 1-Dichloroethene ND<3 X� lenes,total 41 <br /> cis-1,2-Dichloroethene ND<3 <br /> trans-I 2-Dichloroethene Nl:><3 <br />' 1,2-Dichloropropane ND<3 <br /> 1,3-Dichloropropane ND<3 <br /> 2,2-Dichloropropane ND<3 Comments 1 <br /> 1,1-Dichloropropene ND<3 Surrogate Reco%eries{%) <br />' cis-1,3-Dichioropropene ND<3 Dibromofluoromethane 98 <br /> trans-l,3-Dichloropropene ND<3 Toluene-e8 105 <br /> Ethylene dibromide ND<3 4-Bromofluorobenzene 126 <br />' water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/wipe ND means not detected aboi a the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4 methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (1)liquid sample that contains greater than --5 No] % <br />' sediment,6)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattem of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 / Edward Hamilton,Lab Director <br /> 1 <br />