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110 Second Avenue South,##07,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 hhp_//www mccamnbell corn E-mail main@mccampbell com <br /> • <br /> IAdvanced GeoEnvironmental Client Project ID Newfield Property Date Sampled 01/26/99 <br /> 4005 North Wilson Way Date Received 01/28/99 <br /> Stockton,CA 95205 CIient Contact Kevin McKibben Date Extracted 01/28/99 <br /> 1 Client P O Date Analyzed 0I/28/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 02460 <br /> I Client ID MW6/1-26-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ND Eihylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzene ND <br /> Bromodichlorometbane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chlonde"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone" ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone 15 ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Naphthalene NDS <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorohenzene ND St%Tene' ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether` ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene 25 <br /> Chloromethane ND Toluene ND <br /> 2-Chlorotoluene ND 1,2,3-Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 12,4-Tnchlorobenzene ND <br /> I Dtbromochloromethane ND 1,11-Tnchlorocthane ND <br /> 12-Dlbrom0-3-chloropropane ND 1 1 2-Tnchloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Tnchlorofluoromethane ND <br /> I 3,3 Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethyibenzene ND <br /> Dichlorodifluoromethane ND 13,5-Tnmethyibenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate"I ND <br /> 1,2-Dichloroethane 48 Vinyl Chloride`° ND <br /> 1 1-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> I 12-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Rem cries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 99 <br /> trans-l,3-Dichloropropene ND Toluene-d8 98 <br /> Ethylene dibromrde ND I 4-Bromofluorobenzene 89 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> . 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyse not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> I pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethane,(o)dimethylbenzenes <br /> DHS Certification No 1644 i 77 Edward Hamilton, Lab Director <br />