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110 Second Avenue South,##D7,Pacheco CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> I24 hM2//www mccampbell com E-mail main@mccampbell com
<br /> Advanced GeoEnvironmental CIient Project ID Newfield Property Date Sampled 01/26/99
<br /> 4005 North Wilson Way
<br /> Date Received 01/28/99
<br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 01/28/99
<br /> Client P O Date Analyzed 01/28/99
<br /> I Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 02461
<br /> Client ID MW7/1-26-99
<br /> Matrix W
<br /> Compound Concentration* Compound Concentration*
<br /> Acetone" ND Ethylbenzene ND
<br /> Benzene ND Hexachlorobutadiene ND
<br /> Bromobenzene ND Iodomethane ND
<br /> Bromochloromethane ND Isopropylbenzene ND
<br /> Bromodichloromethane ND p-Isopropyl toluene ND
<br /> Bromoform ND Methyl butyl ketone" ND
<br /> Bromomcthane ND Methylene Chloride") ND
<br /> I n-Butyl benzene ND Methyl ethyl ketone" ND
<br /> sec-Butyl benzene ND Methyl isobutyl ketone`B ND
<br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE)
<br /> Carbon Disulfide ND Naphthalene ND<5
<br /> Carbon Tetrachloride ND n Propyl benzene ND
<br /> Chlorobenzene ND Styrene' ND
<br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND
<br /> 2-Chloroethyl Vinyl Ether ND 1,1,2,2-Tetrachloroethane ND
<br /> I Chloroform ND Tetrachloroethene 15
<br /> Chloromethane ND Toluene' ND
<br /> 2-Chlorotoluene ND 1,2,3-Tnchlorobenzene ND
<br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND
<br /> Dibromochloromethane ND 1,1,1-Tnchloroethane ND
<br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Tnchloroethane ND
<br /> Dibromomethane ND Tnchloroethene 12
<br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND
<br /> 1,3-Dichlorobenzene ND 1,2,3-Tnchl oropropane ND
<br /> 1,4-Dichlorobenzene ND 1,2 4-Tnmethylbenzene ND
<br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND
<br /> 1,1-Dichloroethane ND Vinyl Acetate"IND
<br /> 1,2-Dichloroethane ND Vinyl Chlonde'" ND
<br /> 13-Dichloroethene ND Xylenes,total ND
<br /> cis-1,2-Dichloroethene ND
<br /> trans-l,2-Dichloroethene ND
<br /> 1,2-Dichloropropane ND
<br /> 1,3-Dichloropropane ND
<br /> 2,2-Dichloropropane ND Comments t
<br /> 1,1-Dichloropropene ND Surrogate Reco%eries(%)
<br />' cis-1,3-Dichloropropene ND Dibromofluoromethane 102
<br /> trans-1,3-Dichloropropene ND Toluene-d8 99
<br /> Ethylene dibromide ND 4 Bromofluorobenzene 92
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> Reporting limits unless otherwise stated water samples 1 0 ug/L., %apor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes
<br /> 0 Zug/wipe ND means not detected above the reporttng limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropyl acetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment,6}sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for
<br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 fi! Edward Hamilton, Lab Director
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