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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Chcnt Applied Earth Sciences, Inc Service Request X2400183 <br /> Ploject Canteen Corp/AGE-NC-99-0612 Date Extiacted 03/02/2004 <br /> le Mat]tx Water Date Analyzed 03/02/2004 <br /> Lab Conti of Spike/Duplicate Lab Control Spike Summary <br /> TPH as Gasoline(GAO) <br /> Exti action Method EPA 5030E Units ug/L <br /> Analysis Method 8015 GRO Basis NA <br /> Level Low <br /> Extraction Lot XWG0400300 <br /> Lab Control Sample Duplicate Lab Control Sample <br /> XWG0400300-1 XWG0400300-2 <br /> Lab Control Spike Duplicate Lab Control Spike <br /> %Rec RPD <br /> Analyte Name Result Expected %Rec Result Expected %Rec Limits RPD Limit <br /> C6 -C10 GRO 1060 1000 106 1090 1000 109 70-130 3 30 <br /> I <br /> 0s Wigged is ith an tsterisk(")Indic tte t Hues outside control ci iteria <br /> IPercent recovenes Ind relative percent dtficrences(RPD)-ire detarramcd by the soRware usury values in the calculation which have not been founded <br /> IPanted 03/09/2004 08 44 36 Form 3C-OrgatnL Page 1 of 1 <br /> L 15TF4LTFi1CRYsTA1.RPTTorm3D1,C rpt Superset Reference RR4347 <br /> 5 <br />