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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Client Applied Earth.Sciences, Inc Service Request X2400183 <br /> Pi olect Canteen Corp/AGE-NC-99-0612 Date Extracted 03/03/2004 <br /> ple Matr>x Water Date Analyzed 03/03/2004 <br /> L,tb Conti of Spike/Duplicate Lab Control Spike Summary <br /> TPH as Gasoline(GRO) <br /> Eesti action Method EPA 5030B Units ug/L <br /> Analysis Mcthod 8015 GRO Basis NA <br /> Levee Low <br /> Extraction Lot XWG0400311 <br /> Lab Control Sample Duplicate Lab Control Sample <br /> I XWG0400311-1 XW G0400311-2 <br /> Lab Control Spike Duplicate Lab Control Spike u <br /> /oRec RPD <br /> Analvte Name Result Expected %Rei. Result Eapectf.d %Ret_ Limits RPD Limit <br /> IC6 - C10 GRO 888 1000 89 1090 1000 109 70-130 20 30 <br /> I <br /> I <br /> I <br /> I <br /> I <br /> I <br /> *I fl egged Hcth rn cstei tsk(")tudtc cte i,iiuec outsicie coati of cntettl <br /> Pei cent recoveries vtd ielattve hetcent differences(RPD)Ire detennmed by the sofriv-ire using values in the calculation Much hive not been i ounded <br /> Printed 03/09/2004 08 44 40 Form 3C-Orgatuc Page l of 1 <br />{ L\=-ALTHICRYS'tAL RPT-Tom,3DLC rpt SnperSet Reference RR4347 <br />