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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth Sciences, Inc Service Request L2400548 <br /> I Protect Canteen Corp/AGE-NC-99-0612 Date Collected lo02/24/2004 <br /> pie Matrix Water Date Received 02/26/2004 <br /> Volatile Organic Compounds <br /> ISample Name MW 13A/022404 Units ug/L <br /> Lab Code L2400548-005 Basis NA <br /> Extraction Method EPA 503011 Level Low <br /> IAnalysis Method 8260B <br /> Dilution Date Date Extraction <br /> IAnalyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> Benzene 096 050 019 1 03/08/04 03/08/04 LWG04-01005 <br /> 1,2-Dibromoethane(EDB) ND U 050 017 1 03/08/04 03/08/04 LWG0401005 <br /> 1,2-Dichloroethane(EDC) ND U 050 024 1 03/08/04 03/08/04 LWG0401005 <br /> Ethylbenzene 0 74 050 018 1 03/08/04 03/08/04 LWG0401005 <br /> Toluene 3 6 050 0 17 1 03/08/04 03/08/04 LWG0401005 <br /> o-Xylene 12 050 0 13 1 03/08/04 03/08/04 LWG0401005 <br /> m,p-Xylenes 2 8 10 027 1 03/08/04 03/08/04 LWG0401005 <br /> Diisopropyl Ether ND U 2 0 035 1 03/08/04 03/08/04 LWG0401005 <br /> tert-Butyl Ethyl Ether ND U 2 0 0 28 1 03/08/04 03/08/04 LWG0401005 <br /> Itert-Amyl Methyl Ether ND U 2 0 032 1 03/08/04 03/08/04 LWG0401005 <br /> Methyl tert-Butyl Ether ND U 10 031 1 03/08/04 03/08/04 LWG0401005 <br /> -Butyl Alcohol ND U 20 3 3 1 03/08/04 03/08/04 LWG0401005 <br /> IControl Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> IDibromofluoromethane 119 72-134 03/08/04 Acceptable <br /> Toluene-d8 104 82-118 03/08/04 Acceptable <br /> 4-Bromofluorobenzene 94 71-119 03/08/04 Acceptable <br /> I <br /> I <br /> 9ments <br /> 9 <br /> Printed 03/12/2004 15 48 08 Form I-Organic Page 1 of 1 <br /> P 1STEALTHICRYSTAL RPTTormlm rpt Merged Superset Reference RR5281 <br />