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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth Sciences,Inc Service Request L2400548 <br /> IProtect Canteen Corp/AGE-NC-99-0612 Date Collected 02/24/2004 <br /> Ople Matrix Water Date Received 02/26/2004 <br /> I <br /> Volatile Organic Compounds <br /> ISample Name MW 13B/022404 Units ug/L <br /> Lab Code L2400548-006 Basis NA <br /> Extraction Method EPA 5030B Level Low <br /> IAnalysis Method 8260B <br /> Dilution Date Date Extraction <br /> IAnalyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> Benzene ND U 050 019 1 03/08/04 03/08/04 LWG0401005 <br /> 1,2-Dibromoethane(EDS) ND U 050 017 1 03/08/04 03/08/04 LWG0401005 <br /> 1,2-Dichloroethane(EDC) ND U 050 024 1 03/08/04 03/08/04 LWG0401005 <br /> Ethylbenzene ND U 050 0 18 1 03/08/04 03/08/04 LWG0401005 <br /> Toluene ND U 050 0 17 1 03/08/04 03/08/04 LWG0401005 <br /> o-Xylene ND U 050 0 13 1 03/08/04 03/08/04 LWG0401005 <br /> m,p-Xylenes ND U 10 027 1 03/08/04 03/08/04 LWG0401005 <br /> Dnsopropyl Ether ND U 20 035 1 03/08/04 03/08/04 LWG0401005 <br /> tert-Butyl Ethyl Ether ND U 20 028 1 03/08/04 03/08/04 LWG0401005 <br /> tert-Amyl Methyl Ether ND U 20 032 1 03/08/04 03/08/04 LWG0401005 <br /> Methyl tert-Butyl Ether ND U 1 0 031 1 03/08/04 03/08/04 LWG0401005 <br /> Butyl Alcohol ND U 20 33 1 03/08/04 03/08/04 LWG0401005 <br /> Control Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> Dibromofluoromethane 121 72-134 03/08/04 Acceptable <br /> Toluene-d8 106 82-118 03/08/04 Acceptable <br /> 4-Bromofluorobenzene 91 71-119 03/08/04 Acceptable <br /> I <br /> I <br /> Comments <br /> 10 <br /> Printed 03/12/2004 15 48 12 Farm I-Organic Page 1 of 1 <br /> 26P 1STEALTH\CRYSTAL RPT�Formlrnrpt Merged Superset Reference RR$281 <br />