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l 1534 Willow Pass Road,Pittsburg,CA 94565-1701 M c C a m p b e I l Analytic al, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 ,%at "When Quality Countsrr http://www.mccampbell.com/E-mail:main@mccmVbell.com Quality Control Report Client: Clean Harbors WorkOrder: 2006B 17 Date Prepared: 06/27/2020 BatchID: 200873 Date Analyzed: 06/27/2020 Extraction Method: SW5030B Instrument: GC18 Analytical Method: SW8260B Matrix: Water Unit: gg/L Project: 2003281924;Quest Industries Sample ID: MB/LCS/LCSD-200873 QC Summary Report for SW8260B Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD Result Result Val %REC %REC Limits Limit Acetone 39.4 38.7 40 99 97 32-138 1.93 20 tert-Amyl methyl ether(TAME) 3.96 4.05 4 99 101 62-119 2.12 20 Benzene 4.32 4.52 4 108 113 71-126 4.55 20 Bromobenzene 3.69 3.86 4 92 96 66-117 4.30 20 Bromochloromethane 4.24 4.33 4 106 108 67-124 1.92 20 Bromodichloromethane 4.17 4.30 4 104 108 63-119 3.11 20 Bromoform 3.62 3.74 4 90 93 46-117 3.27 20 Bromomethane 4.32 4.46 4 108 112 32-171 3.33 20 2-Butanone(MEK) 15.6 15.5 16 98 97 48-136 0.664 20 t-Butyl alcohol(TBA) 15.4 15.3 16 96 95 40-131 0.834 20 n-Butyl benzene 4.28 4.46 4 107 111 75-125 4.14 20 sec-Butyl benzene 4.28 4.52 4 107 113 72-120 5.42 20 tert-Butyl benzene 3.89 4.11 4 97 103 63-118 5.37 20 Carbon Disulfide 4.60 4.85 4 115 121 64-126 5.19 20 Carbon Tetrachloride 4.51 4.76 4 113 119 67-122 5.54 20 Chlorobenzene 4.04 4.18 4 101 104 71-117 3.33 20 Chloroethane 5.23 5.45 4 131 136 53-136 4.02 20 Chloroform 4.34 4.52 4 108 113 67-126 4.08 20 Chloromethane 4.92 5.12 4 123 128 42-148 3.98 20 2-Chlorotoluene 3.95 4.18 4 99 104 70-117 5.59 20 4-Chlorotoluene 3.85 4.01 4 96 100 67-117 4.21 20 Dibromochloromethane 3.77 3.87 4 94 97 52-120 2.43 20 1,2-Dibromo-3-chloropropane 1.34 1.38 2 67 69 38-128 3.05 20 1,2-Dibromoethane(EDB) 1.79 1.82 2 90 91 58-117 1.51 20 Dibromomethane 4.13 4.18 4 103 104 66-120 1.05 20 1,2-Dichlorobenzene 3.80 3.92 4 95 98 71-117 3.01 20 1,3-Dichlorobenzene 3.88 4.02 4 97 100 74-116 3.47 20 1,4-Dichlorobenzene 3.69 3.87 4 92 97 71-115 4.79 20 Dichlorodifluoromethane 4.84 5.05 4 121 126 29-145 4.31 20 1,1-Dichloroethane 4.26 4.48 4 106 112 68-128 5.18 20 1,2-Dichloroethane(1,2-DCA) 4.11 4.21 4 103 105 61-123 2.36 20 1,1-Dichloroethene 4.43 4.65 4 111 116 65-126 4.92 20 cis-1,2-Dichloroethene 4.24 4.40 4 106 110 71-122 3.77 20 trans-1,2-Dichloroethene 4.34 4.57 4 109 114 70-126 5.23 20 1,2-Dichloropropane 4.06 4.22 4 102 105 67-124 3.73 20 1,3-Dichloropropane 3.77 3.78 4 94 94 65-120 0.318 20 2,2-Dichloropropane 4.73 4.90 4 118 122 71-127 3.38 20 1,1-Dichloropropene 4.42 4.66 4 111 117 69-122 5.30 20 (Cont.) CA ELAP 1644•NELAP 4033ORELAP Page 17 of 31