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l 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> M c C a m p b e I l Analytic al, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> ,%at "When Quality Countsrr http://www.mccampbell.com/E-mail:main@mccmVbell.com <br /> Quality Control Report <br /> Client: Clean Harbors WorkOrder: 2006B 17 <br /> Date Prepared: 06/27/2020 BatchID: 200873 <br /> Date Analyzed: 06/27/2020 Extraction Method: SW5030B <br /> Instrument: GC18 Analytical Method: SW8260B <br /> Matrix: Water Unit: gg/L <br /> Project: 2003281924;Quest Industries Sample ID: MB/LCS/LCSD-200873 <br /> QC Summary Report for SW8260B <br /> Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD <br /> Result Result Val %REC %REC Limits Limit <br /> cis-1,3-Dichloropropene 3.81 3.92 4 95 98 63-119 2.80 20 <br /> trans-1,3-Dichloropropene 3.77 3.90 4 94 97 63-116 3.21 20 <br /> Diisopropyl ether(DIPE) 4.06 4.18 4 102 105 64-128 3.00 20 <br /> Ethylbenzene 4.04 4.26 4 101 106 69-120 5.20 20 <br /> Ethyl tert-butyl ether(ETBE) 3.88 3.99 4 97 100 63-120 2.94 20 <br /> Freon 113 4.52 4.77 4 113 119 67-126 5.46 20 <br /> Hexachlorobutadiene 3.81 4.08 4 95 102 50-140 6.73 20 <br /> Hexachloroethane 3.88 4.08 4 97 102 52-122 4.94 20 <br /> 2-Hexanone 3.26 3.49 4 82 87 39-121 6.68 20 <br /> Isopropyl benzene 4.07 4.35 4 102 109 69-120 6.70 20 <br /> 4-Isopropyl toluene 4.02 4.23 4 101 106 72-122 5.14 20 <br /> Methyl-t-butyl ether(MTBE) 4.03 4.10 4 101 103 60-121 1.79 20 <br /> Methylene chloride 4.02 4.20 4 101 105 40-148 4.39 20 <br /> 4-Methyl-2-pentanone(MIBK) 3.53 3.45 4 88 86 48-115 2.07 20 <br /> Naphthalene 3.70 3.60 4 93 90 62-124 2.80 20 <br /> n-Propyl benzene 4.05 4.30 4 101 108 70-118 6.09 20 <br /> Styrene 3.81 3.92 4 95 98 57-118 2.69 20 <br /> 1,1,1,2-Tetrachloroethane 3.87 4.08 4 97 102 63-117 5.22 20 <br /> 1,1,2,2-Tetrachloroethane 3.48 3.54 4 87 89 60-116 1.77 20 <br /> Tetrachloroethene 4.07 4.28 4 102 107 60-131 5.13 20 <br /> Toluene 4.01 4.20 4 100 105 67-115 4.63 20 <br /> 1,2,3-Trichlorobenzene 3.58 3.51 4 89 88 60-128 1.73 20 <br /> 1,2,4-Trichlorobenzene 3.54 3.66 4 88 91 61-133 3.32 20 <br /> 1,1,1-Trichloroethane 4.33 4.56 4 108 114 67-124 5.04 20 <br /> 1,1,2-Trichloroethane 3.78 3.82 4 95 96 62-117 1.16 20 <br /> Trichloroethene 4.27 4.47 4 107 112 69-120 4.60 20 <br /> Trichlorofluoromethane 4.66 4.94 4 117 123 60-134 5.72 20 <br /> 1,2,3-Trichloropropane 1.92 1.94 2 96 97 56-120 1.50 20 <br /> 1,2,4-Tri methyl benzene 3.89 4.08 4 97 102 67-124 4.66 20 <br /> 1,3,5-Tri methyl benzene 3.95 4.13 4 99 103 69-122 4.32 20 <br /> Vinyl Chloride 2.50 2.61 2 125 131 52-145 4.57 20 <br /> m,p-Xylene 8.01 8.32 8 100 104 67-119 3.76 20 <br /> o-Xylene 3.92 4.07 4 98 102 68-120 3.70 20 <br /> (Cont.) <br /> CA ELAP 1644•NELAP 4033ORELAP <br /> Page 18 of 31 <br />