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Nov, 12. 2008 4:05PM <br />No, 2067 P. 10 <br />, <br />1534 <br />SmsRoad Pi94565.1701 <br />cCAmgbell AnalyticalInc. wey:yww.ccampbell.tom E-mA-msin@accsmpbell <br />.cgm <br />'When av%liry counts" I Tole hoae:877-252-9262 Fax: 925-252-9269 <br />QC SUMMARY REPORT FOR SW8260B <br />.,n hA-P--- e..ri 0CMafrix: Soil BatchlD: 38900 WorkOrder 08904`15 <br />EPA Method SW82600 <br />Extraction SW6030B <br />Spiked Sample ID: 0810354.009A <br />Analyte <br />Sample <br />m91K9 <br />Spiked <br />mEM9 <br />MS <br />% Rec. <br />MSD <br />% Roo, <br />MS -MSD <br />% RPD <br />LCS <br />% Rec- <br />LCSD <br />% Rec. <br />LCS-LCSD Acceptance Criteria (%) <br />% RPD MS / MSD RPD LOS/LCSD <br />FPD . <br />cert -Am t methyl ether TAME.) <br />ND <br />0.050 <br />94.8 <br />92,1 <br />2.89 <br />98.1 <br />1024.06 <br />60 - 130 <br />30 <br />60-130 <br />30 <br />Benzene <br />ND <br />0.050 <br />111 <br />106 <br />4.43 <br />114 <br />118 <br />2,73 <br />60-130 <br />30 <br />60. 60 <br />30 <br />t -Butyl alcohol (TBA) <br />ND <br />0.25 <br />78.1 <br />74 <br />5.30 <br />89.8 <br />95.5 <br />6.17 <br />60-130 <br />30 <br />60-130 <br />30 <br />Chlorobenzene <br />ND <br />0.050 <br />103 <br />102 <br />0.825 <br />106 <br />107 <br />0.948 <br />60- 130 <br />30 <br />60- 130 <br />30 <br />1.2-Dibromoethane EDB <br />ND <br />0.050 <br />119 <br />120 <br />1.37 <br />123 <br />125 <br />1.61 <br />60- 130 <br />30 <br />60-130 <br />30 <br />1,2-Dichloroethanc 1.2-0CA) <br />ND <br />0.050 <br />92.1 <br />91.4 <br />0.771 <br />1 97 <br />99.6 <br />2.64 <br />60- 130 <br />30 <br />60-130 <br />30 <br />1.1-Dichloroethene <br />ND <br />0.050 <br />89.6 <br />85.3 <br />4.86 <br />1 93.7 <br />96.5 <br />2.95 <br />60-130 <br />30 <br />60-130 <br />30 <br />Diisopropyl ether DIPE) <br />NO <br />0.050 <br />86.6 <br />85-5 <br />1.32 <br />87.3 <br />91.4 <br />4.54 <br />60-130 <br />30 <br />60-130 <br />30 <br />Ethyl cert -butyl ether (ETSE) <br />ND <br />0.050 <br />93.3 <br />91.8 <br />1.53 <br />97.4 <br />99.9 <br />2.54 <br />60- 130 <br />30 <br />60. 130 <br />30 <br />Methyl -t -butyl other (MTBE) <br />ND <br />0.050 <br />82 <br />79.9 <br />2.52 <br />86.3 <br />88.2 <br />2.17 <br />60- 130 <br />30 <br />60-130 <br />30 <br />Toluene <br />ND <br />0.050 <br />113 <br />113 <br />0 <br />115 <br />119 <br />3,36 <br />60-130 <br />30 <br />60-130 <br />30 <br />Triehloroethene <br />NA <br />0.050 <br />116 <br />112 <br />3.20 <br />118 <br />121 <br />2.01 <br />60. 130 <br />30 <br />60-130 <br />30 <br />°/SSI: <br />80 <br />0.12 <br />80 <br />1 80 <br />0 <br />82 <br />83 <br />0.444 <br />70- 130 <br />30 <br />10-130 <br />30 <br />°/=2: <br />96 <br />0.12 <br />99 <br />94 <br />0 <br />92 <br />93 <br />1.02 <br />70- 130 <br />30 <br />70 - 130 <br />30 <br />°/S33: <br />99 <br />0.012 <br />103 <br />106 <br />3.00 <br />1 i 1 <br />109 <br />2.53 <br />70-130 <br />30 <br />70 - 130 <br />30 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NONE <br />BATCH 36900 SUMMARY <br />Lab ID Dale Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Dale Analyzed <br />081041T001A 10/16/08 9:410 AM 10/17108 LO/17/08 5:39 PM <br />MS = Metrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample. LCSD = Laboratory Contra Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery a too ` (MS -Sample) I (Amount Spiked); RPD =100 - (AAS - MSD) I ((MS + MSD) / 2). <br />M$ / MSD spike recoveries and / or 9ARPD may fall outside of laboratory acceptance criteria due to one or more 01 the following reasons: e) the sample is Inhomogenoua AND <br />Contains algnlflcent concentrations of analyte relative to the amount spited, or b) the spiked samp]as matrix Interferes with the spike recovery. <br />N/A n not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration In sample exceeds spike amount for son matrix or exceeds 2x spike amount forwater matrix or sample diluted due to high matrix or analyse content. <br />Laticiratory extraction solvents such as methylene chbride and acetone may occasionally appear In the method blank at low levels. <br />DHS.ELAP Certification 1644 `W-- QkQC Officer <br />