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Li <br />Nov, 12. 2008 4:05PM , <br />No, 2067 P. 11 <br />cCa �pbell Analytical, TIIC. 1534 necawPossRoad PFinafl:waEotsburg. CA 9x565-1701 <br />bel <br />Web: www.mecampbeli.com &mail: msie(�accamp6otl.wna <br />'WhenoualitvCounts" Telephone! 811-252-9262 Fsx935-252.9369 <br />QC SUMMARY REPORT FOR 6020A <br />W.O. Sample Matrix, Soil QC Matrix: Soil WorkOrder 0810415 <br />EPA Method 6020A <br />Extraction SW305013 <br />BatchlD: 38838 <br />Spiked Sample ID 0610274-001A <br />Analyte <br />Sample <br />nVKg <br />Spiked <br />mg/Kg <br />MS <br />1/6 Rec. <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />Spiked <br />ntg/i(g <br />LCS <br />% Rec. <br />LCSD <br />°% Rea <br />LCS-LCSD <br />% RPD <br />Acceptance Criteria (%) <br />MS / MSD RPD LCS/LCSO <br />RPD <br />Antimony <br />0.56 <br />50 <br />97.8 <br />101 <br />2.95 <br />10 <br />110 <br />109 <br />0.898 <br />70-130 <br />20 <br />80-120 <br />20 <br />Arsenio <br />2.6 <br />50 <br />96.6 <br />L 101 <br />3.74 <br />10 <br />97.2 <br />101 <br />3.53 <br />70-130 <br />20 <br />80- 120 <br />20 <br />Barium <br />49 <br />500 <br />98.7 <br />103 <br />4.25 <br />100 <br />100 <br />100 <br />0 <br />70-130 <br />20 <br />SO- 120 <br />20 <br />Iletyllium <br />ND <br />50 <br />103 <br />108 <br />3,96 <br />10 <br />110 <br />112 <br />1,26 <br />70- 130 <br />20 <br />0 <br />20 <br />Cadmium <br />3.8 <br />50 <br />96.8 <br />99.1 <br />2.18 <br />10 <br />101 <br />101 <br />0 <br />70-130 <br />20 <br />80,120 <br />20 <br />Chromium <br />11 <br />50 <br />89.7 <br />93.1 <br />3.00 <br />10 <br />97.6 <br />98.3 <br />0,674 <br />70-130 <br />20 <br />0 <br />r80, <br />20 <br />Cobalt <br />2.7 <br />50 <br />92.7 <br />96.2 <br />3.47 <br />t 0 <br />91.9 <br />98.5 <br />0,621 <br />10-130 <br />20 <br />0 <br />20 <br />Copper <br />28 <br />50 <br />87.5 <br />92.6 <br />3.51 <br />10 <br />92.6 <br />90.7 <br />2.11 <br />70-110 <br />20 <br />80- 120 <br />20 <br />Lead <br />22 <br />50 <br />97.9 <br />102 <br />3,03 <br />10 <br />100 <br />101 <br />1.08 <br />70-130 <br />20 <br />80- 120 <br />20 <br />Mercury <br />ND <br />1.25 <br />102 <br />107 <br />4.29 <br />0.25 <br />106 <br />109 <br />3.08 <br />70 - 130 <br />20 <br />80- 120 <br />20 <br />Molybdenum <br />1.6 <br />50 <br />94.3 <br />98.1 <br />3.82 <br />10 <br />1 97 <br />99.3 <br />2.35 <br />70-130 <br />20 <br />80-120 <br />20 <br />Nickel <br />12 <br />50 <br />90.4 <br />1 94.2 <br />3.24 <br />10 <br />93.6 <br />95.5 <br />2.01 <br />70-130 1 <br />20 <br />go- 120 <br />20 <br />Selenium <br />ND <br />50 <br />99.8 <br />102 <br />2.08 <br />10 <br />104 <br />103 <br />0.290 <br />70-130 <br />20 <br />SO- 120 <br />20 <br />Silver <br />ND <br />50 <br />99,4 <br />103 <br />3.17 <br />10 <br />98.8 <br />99.7 <br />0.937 <br />70-130 <br />20 <br />80-120 <br />20 <br />Thallium <br />ND <br />50 <br />94 <br />96.4 <br />2.59 <br />10 <br />92.8 <br />94 <br />1.31 <br />70-130 <br />20 <br />SO- 120 <br />20 <br />Vanadium <br />15 <br />50 <br />90.6 <br />94.8 <br />3.40 <br />10 <br />98.2 <br />99.1 <br />0.963 <br />70-130 <br />20 <br />SO- 120 <br />20 <br />Zinc <br />120 <br />500 <br />100 <br />105 <br />3.63 <br />100 <br />102 <br />103 <br />0.683 <br />70-130 <br />20 <br />80-120 <br />20 <br />%SS <br />104 <br />250 <br />104 <br />d08 <br />3.96 <br />250 <br />104 <br />105 <br />1 1.76 <br />70- 130 <br />20 <br />70-130 <br />20 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NON£ <br />t3ATCH 2000 SUMMARY <br />Lab ID Date Sampled Dale Extracted Dale Analyzed Lab ID Date Sampled • Dale Extracted Dale Analyzed <br />0810415-OOIA 10/16/08 9:40 AM 10/17/08 10/20/08 7:33 PM 0810415-OOIA 10/16/08 9:40 AM 10/17/08 10/21/08 6:10 PM <br />1 = Matrix Spike: MSD = Matrix Spike Duplicate; LCS � Laboratory Control Semple; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />Recovery = 100 • (MSSamplo) / (Amount Spiked); RPD a 100 ' (MS - MSD) / ((MS + MSD) / 2). <br />MSD spike recoveries and / or %RPD may rail outside of laboratory acceptance Criteria due to One or more of the following reasons: a) the sample Is Inhomogenous <br />10 contains significant concentrations or analyte relative to the amount spiked, or b) the spiked sample's matrix Interferes with the spike recovery. <br />k = not applicable to We method. <br />t = analyte concentration In sample exceeds spice amount for gob matrix or exceeds 2x spike amount for water m*Vk or sample diluted due to high matrix Or analyte <br />DHS BLAP Certificadon 1644 <br />Op- OA/QC Officer <br />