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Nov, 12. 2008 4:05PM <br />No, 2067 P. 12 <br />cCamoblill Analytical, Ince 1534 Willow pall -Pass om !'&ma0g,CA 96563-1101 <br />cI <br />Web:..,wtiv.mRamp6elLcom &mail:mainrgmccampbell.com <br />"WhenQualityCounts" Tele hone: 877-252-9262 Fax:925-252-9269 <br />QC SY7MVf"Y REPORT FOR SW8015B <br />nr. UnIAY• CWl . ' BatchtD: 38845 <br />WorkOrder 0810415 <br />BATCH 38845 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date 2)dracted Date Analyzed <br />0810415-OOIA 10/16/08 9:40 AM 10/17/08 10/24/08 4:34 AM <br />MS = Matrix Spike; MSD m Matrix $pike Duplicate; LOS = Laboratory Control Sample; LCSD = Laboratory Control Sample DupllcaLe; RPO = Rslalive Percent DftiadOO. <br />% Recovery w 100 ' (Ma -Sample) / (Amount Spiked); RPD = too a (MS - MSD) / ((MS + MSD) 12). <br />MS I MSD spike recoveries an4 / or %RPD may fall outside of laboratory acceptance criteria due to one Oe more of the totiov&g reasons: a) the sample is inhomogenous AHP <br />contains atgniticant coneenUauons of analyte ralallve to the amount spiked, or b) the spiked samples matrix interferes with the apike recovery. <br />WA a not enough sample to perform matrix spike and matrix spike duplicate. <br />NR a anawt concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water ma(rlx Or sample diluted due to high matrix or arta a content. <br />DHS BLAP Certification 1644 ov, QA/QC Officer <br />EPA Method SW8016E Extraction SW3550C <br />Spiked Sample ID: 0810356.002A <br />Sample Spiked MS <br />MSD <br />MS -MSD <br />LCS <br />LCSD <br />LCS-LCSD Aeeeptancn Criteria (%} <br />Analyte <br />mg/K9 "11<9 % Rec. <br />% Rec. <br />% RPD <br />% Rec. <br />% Rec. <br />% RPD MS J MSD RPD LCSS/L.CSD RPD <br />TPH-Diesel CIO,C23) <br />ND 20 116 <br />116 <br />0 <br />106 <br />106 <br />0 70 - 130 30 70-130 30 <br />MOSS, <br />106 50 1 1 I <br />111 <br />0 <br />100 <br />100 <br />0 70 • 130 30 70- 130 30 <br />All target compounds in <br />the Method Blank of this extraction batch were ND less than the <br />method RL With the following exceptions: <br />NONE <br />BATCH 38845 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date 2)dracted Date Analyzed <br />0810415-OOIA 10/16/08 9:40 AM 10/17/08 10/24/08 4:34 AM <br />MS = Matrix Spike; MSD m Matrix $pike Duplicate; LOS = Laboratory Control Sample; LCSD = Laboratory Control Sample DupllcaLe; RPO = Rslalive Percent DftiadOO. <br />% Recovery w 100 ' (Ma -Sample) / (Amount Spiked); RPD = too a (MS - MSD) / ((MS + MSD) 12). <br />MS I MSD spike recoveries an4 / or %RPD may fall outside of laboratory acceptance criteria due to one Oe more of the totiov&g reasons: a) the sample is inhomogenous AHP <br />contains atgniticant coneenUauons of analyte ralallve to the amount spiked, or b) the spiked samples matrix interferes with the apike recovery. <br />WA a not enough sample to perform matrix spike and matrix spike duplicate. <br />NR a anawt concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water ma(rlx Or sample diluted due to high matrix or arta a content. <br />DHS BLAP Certification 1644 ov, QA/QC Officer <br />