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AIR, WATER arid HAZARDOUS WASTE LABORATORY CERTIFIED by CALIFORNIA DEPT of HEALTH SERVICES <br />. * 0 <br />CCAS -NAPA SAMPLE DESCRIPTION: <br />Instrument Blank for 05/03/91 MSD#1 <br />Compound Analyzed Detection Limit Concentration <br />in mg/kg (PQL)* in mg/kg <br />------------------------------------------------------------------------ <br />Coast -to- <br />Coast -to -Coast <br />not <br />Lab Number: 805031 <br />Coast <br />Analytical Services, <br />Inc. <br />Collected: <br />Analytical <br />141 Suburban Road , Suite <br />C-4 <br />Received: <br />Services <br />San Luis Obispo, California <br />93401 <br />Tested: 05/03/91 <br />1,2-Dichloroethane (EDC) <br />(805) 543-2553 <br />not <br />Collected by: <br />Ethylene Dibromide (EDB) <br />FUEL FINGERPRINT <br />ANALYSIS <br />found <br />CAL DNS (TPH Draft) Method <br />& EPA Method 8240/8260-(GC/MS) <br />Extracted by EPA Method 5030 <br />(purge -and -trap)** <br />CCAS -NAPA SAMPLE DESCRIPTION: <br />Instrument Blank for 05/03/91 MSD#1 <br />Compound Analyzed Detection Limit Concentration <br />in mg/kg (PQL)* in mg/kg <br />------------------------------------------------------------------------ <br />BTX as a Percent of Total Fuel <br />n/a <br />Percent Surrogate Recoveries 103/101/106 <br />*(Practical Quantitation Limit) <br />**Soils sonicated during extraction <br />Constituents reported as "not found" would have been reported if present <br />at or above the listed practical quantitation limit. <br />Respectfully submitted, <br />�/� <br />CO S -to-COAs NALYTICAL SERVICES <br />ve?g � -1 r' <br />Mary H licek, Ph.D. <br />President <br />MSD #1-5/06 <br />605031FS1.wr1/FFP72 <br />MH/hc/gb/hc <br />Benzene <br />0.001 <br />not <br />found <br />Toluene <br />0.001 <br />not <br />found <br />Ethylbenzene <br />0.001 <br />not <br />found <br />Xylenes <br />0.001 <br />not <br />found <br />1,2-Dichloroethane (EDC) <br />0.001 <br />not <br />found <br />Ethylene Dibromide (EDB) <br />0.001 <br />not <br />found <br />------------------------------------------------------------------------ <br />Total Purgeable Petroleum Hydrocarbons <br />(Gasoline) ........................... <br />0.1 <br />not <br />found <br />(Diesel #2,Jet Fuel, Kerosene, <br />Stoddard Solvent, Mineral Spirits) .. <br />0.1 <br />not <br />found <br />BTX as a Percent of Total Fuel <br />n/a <br />Percent Surrogate Recoveries 103/101/106 <br />*(Practical Quantitation Limit) <br />**Soils sonicated during extraction <br />Constituents reported as "not found" would have been reported if present <br />at or above the listed practical quantitation limit. <br />Respectfully submitted, <br />�/� <br />CO S -to-COAs NALYTICAL SERVICES <br />ve?g � -1 r' <br />Mary H licek, Ph.D. <br />President <br />MSD #1-5/06 <br />605031FS1.wr1/FFP72 <br />MH/hc/gb/hc <br />