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AIR, WATER and HAZARDOUS WASTE -LABORATORY CERTIFIED by CALIFORNTAMDEPT of HEALTH SERVICES <br />Percent Surrogate Recoveries 105/100/118 <br />*Practical Quantitation Limit <br />**Soils sonicated during extraction <br />Constituents reported as "not found" would have been reported if present <br />at or above the listed practical quantitation limit. <br />Respectfully submitted, <br />COAST-to-CGtZ <br />T ANALYTICAL SERVICES <br />, <br />Mary avlicek Ph.D. <br />President <br />MSD #1-5/06 <br />QS05031G.wr1/FFP71 <br />MH/hc/gb/hc <br />Coast -to- <br />Coast -to -Coast <br />Lab Number: <br />QS05031 <br />Coast <br />Analytical Services, Inc. <br />Collected: <br />Analytical <br />141 <br />Suburban Road , Suite C-4 <br />Received: <br />Services <br />San Luis Obispo, California 93401 <br />Tested: <br />05/03/91 <br />(805) 543-2553 <br />Collected by: <br />FUEL FINGERPRINT ANALYSIS <br />CAL DHS (TPN Draft) Method & EPA Method 8240/8260-(GC/MS) <br />Extracted by EPA Method 5030 (purge -and -trap)** <br />CCAS -NAPA <br />SAMPLE DESCRIPTION: <br />Roasted Soil <br />Spiked to 1.42ppm with <br />Super Unleaded Gasoline <br />Compound Analyzed <br />*PQL Expected <br />Actual <br />Percent <br />------------------------------------------------------------------------ <br />mg/kg in mg/kg <br />in mg/kg <br />Recovery <br />Benzene <br />0.001 0.052 <br />0.053 `` <br />102% <br />Toluene <br />0.001 0.16 <br />0.16 <br />100% <br />Ethylbenzene <br />0.001 0.029 <br />0.027 <br />93% <br />Xylenes <br />0.001 0.17 <br />0.15 <br />88% <br />1,2-Dichloroethane <br />(EDC) 0.001 not spiked <br />----- <br />---- <br />Ethylene Dibromide <br />(EDB) 0.001 not spiked <br />----- <br />---- <br />------------------------------------------------------------------------ <br />Total Purgeable Petroleum <br />Hydrocarbons <br />(Gasoline) <br />0.1 1.42 <br />1.50 <br />106% <br />(Diesel #2, Stoddard <br />Solvent, <br />Kerosene, Jet Fuel, <br />Mineral Spirits) not spiked <br />---- <br />---- <br />BTX as a Percent of <br />Total Fuel <br />24% <br />n/a <br />Percent Surrogate Recoveries 105/100/118 <br />*Practical Quantitation Limit <br />**Soils sonicated during extraction <br />Constituents reported as "not found" would have been reported if present <br />at or above the listed practical quantitation limit. <br />Respectfully submitted, <br />COAST-to-CGtZ <br />T ANALYTICAL SERVICES <br />, <br />Mary avlicek Ph.D. <br />President <br />MSD #1-5/06 <br />QS05031G.wr1/FFP71 <br />MH/hc/gb/hc <br />