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110 Second Avenue South, #D7, Pacheco, CA 94553-5560 <br />MCCAMPBELL ANI ALYTIGA,L INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br />:f!www.mccaai2bell.com E-mail: main mccampbell.com <br />Advanced GeoEnvironmental <br />4005 North Wilson Way <br />Stockton, CA 95205 <br />It <br />Client Project Iii: Waterloo Food And <br />Fuel <br />Date Sampled: 02/16199 <br />1 Date Received: 02117199 <br />Client Contact: Bob Marty <br />Date Extracted: 02111-02l22/99 <br />Client P.O: <br />I Date Analyzed: 02117-02122199 <br />Gasoline Range (C6-Cl2) Volatile Hydrocarbons as Gasoline*, with Methyl tert Butyl Ether* & BTEX* <br />EPA methods 5030, modified 8015, and 8020 or 602; Califomia RWQCB (SF Bay Region) method GCM5030) <br />Lab ID <br />Client M <br />Matrix <br />TPH(g)- <br />MTBE <br />Benzene <br />Toluene <br />F- zonehylb <br />Xylenes <br />%Recovery <br />Surrogate <br />03580 <br />SP -6 <br />S <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />99 <br />03581 <br />03582 <br />SP -7 <br />SS -146N :' <br />S <br />S <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />0.017 <br />ND <br />99 <br />99 <br />03583 <br />SS-2-T5N` -' <br />S <br />ND <br />MT <br />ND <br />ND <br />ND <br />TND <br />100 <br />03584 <br />SS -3-75S , <br />S <br />ND <br />ND <br />C ND <br />ND <br />ND <br />ND <br />99 <br />03585 <br />SS -4-T6$ ` ' <br />S <br />ND <br />ND <br />'ND <br />ND <br />ND <br />ND <br />101 <br />l <br />Reporting LindtUnless <br />otherwise stated; ND <br />means not detected above <br />the reporting limit <br />W <br />50 ug1L l <br />5.0 <br />O.S. <br />0.5 <br />0.5 <br />0.5 <br />$ <br />1.0 mg/kg <br />0,05 <br />0.005 <br />0.005 <br />0.005 <br />0.005 <br />' water and vapor samples are reported in ug/L, wipe samples in ugtwipe, soil and sludge samples in mg/kg, and all TCLY and SPLP extracts <br />in uglL <br />f cluttered chromatogram; sample, peak coclutes with surrogate peak <br />`The follovnng descriptions of the TPH chromatogram are cursory in nature and McCampbeli Analytical is not responsible for tbeir <br />interpretation: a) unmodified or weakly modified gasoline is significant, b) heavier gawlme range compounds we significamt(aged <br />gasoline.); e) lighter gasoline range compounds (the most mobile fraction) an significant; d) gasoline range compounds having broad <br />cluomatoBnPhic peaks am significant. biologically altered gasoline?; e) '1PH Pattern that does not appear to be derived from gasoline (7); f) <br />one to a few isolated peaks present; g) atrmrgly aged gasoline or diesel range compotwds are h) lighter than w>etier irntxtiscible <br />siaeen is present; i} liquid le that tkoti -.�5 vol. Si, scdimrnt; j) ra teco8mzable attemsignificant; <br />DHS Certification No. 1644/' Edward Hamilton, Lab Director <br />,JUl 3 1999 <br />V ip -)'MVIENTAL HEAMI <br />PERMIT/ SERVICES <br />