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110 Second Avenue South, #D7, Pacheco, CA 94553-5560 <br />MCCA APBELL ANAL'YUCAL INC. Telephone: 925-798-1620 Fax: 925-798-1622 <br />ho ht Jlwww.mccart►t+bell.com E-mail main@mccampbell.com <br />mccampbell.com <br />Advanced GeciEnviromnental <br />4005 North Wilson Way <br />Stockton, CA 95205 <br />Client Project ID: Waterloo Food And <br />Fuel <br />pate Sampled: 02/36/99 <br />DateReceived: 02/17/99 <br />� <br />Client Contact: Bob Marty <br />Date Extracted; 02/17/99 <br />Client P.O: <br />Date Analyzed: 02/17/99 <br />Lead* <br />EPA analytical methods 6010/200.7,2392* <br />Lab ID <br />Client ID I <br />Matrix <br />Extraction' Lead' <br />I % Recovery <br />Surrogate <br />03580 <br />SP -6 <br />S <br />TTLC <br />10 <br />95 <br />03581 <br />SP -7 <br />S <br />TTLC <br />7.1 <br />97 <br />03582 <br />SS-l-T6N <br />S <br />TTLC <br />9.5 <br />95 <br />03583 <br />j SS -2 -TSN l <br />S <br />TTLC <br />9.6 <br />94 <br />03584 <br />SS -3 -TSS ' I <br />S <br />TTLC <br />7.9 <br />97 <br />03585 <br />SS-4-T6S'- <br />S <br />TTLC <br />! 7.9 <br />93 <br />t <br />I <br />! <br />r <br />1 <br />Reporting Limit unless otherwise <br />stated; ND mems not detected above <br />the repotting limit <br />5 <br />TTLC � <br />3.0 mg/kg <br />W ! <br />TTLC i 0-005 mg/L <br />-- j <br />STLC,TCLF 0.2 mg/L <br />* soil and sludge samples are reported in mglkg, wipe samples in ug/wiwe, and water aamples and all STLC! SPLP / TCLP extracts in mylL <br />'Lead a analysed using EPA method 6010 (ICP)for soih,sludgm, STLC B TCLP extracts and method 239.2 (AA Furnace) for water <br />samples <br />° EPA exvaction methods 1311(TCLP), 30lQ020(wa1er,TTLC), 3M(orga» c nmrnces,TTLC), 3050(solids,TTLC); STLC - CA Title 22 <br />` surrogate diluted out of range; NIA marts surrogate not applicable to this analysis <br />k reporting lirmt raised due matna mterference <br />i) liquid sample that contains greater than --2 vol. % sediment; this sediment it, extracted with the liquid, in accordance with EPA <br />mcthodologice and can eignificandy effect reported metal concentrations. <br />DHS Certification No. 164413 <br />9 J J/ X /,,l Edward Hantilton, Lab Director <br />a:. <br />.JUL 3 0 1999 <br />ENVIRONMENTAL HEALTH <br />PERMIT/SERVICES <br />