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G <br /> MINIMUM VERIFICATI()N LABORATORY ANALYSIS <br /> - METALS PCB <br /> R7 - <br /> Tr�a![C TPH-(i TPH-D RTX& CL HC TOTAL B <br /> CONTENTS 8015 8015 F 9010 LEAD ICAP/ 8270 <br /> 826() 8260 80120 8240 7.120 8230 AES or 8080 <br /> 826() 7421 AA <br /> LEADED GAS X X X X <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> INK F171. X X X X X <br /> PROD Oil. X <br /> CHLOR. X X <br /> SOLVENTS <br /> NONCHLOR X X X <br /> SOLVENTS <br /> WASTE\ X X X X X X <br /> USED OIL <br /> All analyses nhedxxls are designated EPA nhcdhtxh described in EPA SW 846,Third Edition. Tlhose methods not found in <br /> SW 846,are specifically notedbelow.Blow. Refer to die"SW RC B LUF'T Field Manual".Appendix A-20.Table 3-5 for detection <br /> limits of motor vehicle fuels(gasoline and diesel). Refer xr 1-2-3 "Regionad Board Staff Recomnhendations for Initial <br /> Evaluation amid Investigation Of UST•s" for tlx: waste and moU>r Oil dctection luuits. <br /> Detection Limits that remain below the %Icl.. STLC or Allowable Limit or the contaminant in <br /> question will he accepted. however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrtx:arbxnas <br /> .Gasoline.C'JC/F[D(5030)8015 mod or GC/MS 8260 <br /> TPH-D Total Petmleum Hydrocarbon.Dicsel.G RD(3550).8015 mod or GUMS 8260 <br /> BTX&E Benzene.Toluene.Xylene&Ethyl Benzene.GC/PID 8020 or GUMS 8260 <br /> CL HC Chlorinated Hydrocarbon.GC-1HSD 8010,(jC/MS 8240 <br /> TOTAL LEAD Total lead. AA 7420. AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide(DTSC-AB 1803).GC/MS 8240(DISC-LUFD <br /> GC-FID Gas Chroxmato__raphy.Flanhc Ionization Detection <br /> [CAP or AA Inductively Coupled Plasma►Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 700. Metals: Cadmium. Chromium III and VI. Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls.GC/MS 8270 or 8084 <br /> Method 3050 Acid digestion <br /> Method 354(1 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection o><benzene,N.nzene-free w)lvents are to be used. Fused capilkuy columns are <br /> preferred to packed columns:a packed column may be used as a"first cut"with"dirty"samples or once the hydrocarbons have <br /> been characterized and proper QA/AC is followed. <br /> For Drinking water sources.EPA recommends that the 51x►series for volatile organics be used in preference to the 6(11)series <br /> because the detection limits are lower and die QA/Q(;is better. Sample-;exhibiting any level of heavy metal contaunination <br /> may require further arta- ysis. PHS-EHD reconhmends holding dose samples until disposal is indicated. <br /> EH 23(W (Rev 7/1(/92) <br /> J x <br />