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QC Sample Results <br /> Client: HydroChemPSC Job ID: 720-96745-1 <br /> Project/Site: R-1036 Tracy,CA <br /> Method: 8260B/CA LUFTMS - 8260B / CA LUFT MS (Continued) <br /> Lab Sample ID: LCSD 720-277956/6 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 277956 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 101 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 100 60-140 <br /> Toluene-d8(Surr) 101 58-140 <br /> Lab Sample ID: LCSD 720-277956/8 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 277956 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Gasoline Range Organics(GRO) 1000 1080 ug/Kg 108 70-122 2 20 <br /> -C4-C12 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 107 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 103 60-140 <br /> Toluene-d8(Surr) 99 58-140 <br /> Lab Sample ID: 720-96745-1 MS Client Sample ID: R-1036-SOIL-DISPOSAL-1230 <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 277956 Prep Batch: 277971 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Methyl tert-butyl ether ND 47.4 59.8 ug/Kg 126 69-130 <br /> Acetone ND F1 237 530 F1 ug/Kg 224 37-150 <br /> Benzene ND 47.4 51.1 ug/Kg 108 70-130 <br /> Dichlorobromomethane ND 47.4 56.2 ug/Kg 118 64-135 <br /> Bromobenzene ND F1 47.4 63.8 F1 ug/Kg 134 70-130 <br /> Chlorobromomethane ND 47.4 54.1 ug/Kg 114 65-130 <br /> Bromoform ND 47.4 58.1 ug/Kg 122 58-132 <br /> Bromomethane ND 47.4 49.0 ug/Kg 103 56-130 <br /> 2-Butanone(MEK) ND 237 229 ug/Kg 97 41-150 <br /> n-Butylbenzene ND 47.4 44.2 ug/Kg 93 60-145 <br /> sec-Butylbenzene ND 47.4 49.9 ug/Kg 105 64-137 <br /> tert-Butyl benzene ND 47.4 53.7 ug/Kg 113 63-134 <br /> Carbon disulfide ND 47.4 49.0 ug/Kg 103 10-150 <br /> Carbon tetrachloride ND 47.4 53.6 ug/Kg 113 54.130 <br /> Chlorobenzene ND 47.4 51.4 ug/Kg 108 70-130 <br /> Chloroethane ND 47.4 56.8 ug/Kg 120 61-130 <br /> Chloroform ND 47.4 52.6 ug/Kg 111 67-130 <br /> Chloromethane ND 47.4 56.8 ug/Kg 120 50-131 <br /> 2-Chlorotoluene ND 47.4 58.5 ug/Kg 123 70-130 <br /> 4-Chlorotoluene ND 47.4 57.5 ug/Kg 121 70-130 <br /> Chlorodibromomethane ND 47.4 56.1 ug/Kg 118 60-141 <br /> 1,2-Dichlorobenzene ND 47.4 52.9 ug/Kg 111 70-130 <br /> 1,3-Dichlorobenzene ND 47.4 53.1 ug/Kg 112 70-130 <br /> 1,4-Dichlorobenzene ND 47.4 54.2 ug/Kg 114 70-130 <br /> 1,3-Dichloropropane ND 47.4 55.7 ug/Kg 117 70-130 <br /> 1,1-Dichloropropene ND 47.4 49.1 ug/Kg 104 67-130 <br /> Eurofins TestAmerica, Pleasanton <br /> Page 15 of 49 1/8/2020 <br />