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QC Sample Results <br /> Client: HydroChemPSC Job ID: 720-96745-1 <br /> Project/Site: R-1036 Tracy,CA <br /> Method: 8260B/CA LUFTMS - 8260B /CA LUFT MS (Continued) <br /> Lab Sample ID: 720-96745-1 MS Client Sample ID: R-1036-SOIL-DISPOSAL-1230 <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 277956 Prep Batch: 277971 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,2-Dibromo-3-Ch loropropane ND F1 47.4 68.2 F1 ug/Kg 144 57.130 <br /> Ethylene Dibromide ND 47.4 54.0 ug/Kg 114 66-135 <br /> Dibromomethane ND 47.4 55.5 ug/Kg 117 65-131 <br /> Dichlorodifluoromethane ND 47.4 55.3 ug/Kg 117 38-130 <br /> 1,1-Dichloroethane ND 47.4 52.9 ug/Kg 112 67.130 <br /> 1,2-Dichloroethane ND 47.4 55.8 ug/Kg 118 70-130 <br /> 1,1-Dichloroethene ND 47.4 53.7 ug/Kg 113 64-130 <br /> cis-1,2-Dichloroethene ND 47.4 54.2 ug/Kg 114 68-131 <br /> trans-1,2-Dichloroethene ND 47.4 52.2 ug/Kg 110 70-130 <br /> 1,2-Dichloropropane ND 47.4 55.4 ug/Kg 117 65-133 <br /> cis-1,3-Dichloropropene ND 47.4 50.6 ug/Kg 107 46-139 <br /> trans-1,3-Dichloropropene ND 47.4 51.2 ug/Kg 108 55-131 <br /> Ethylbenzene ND 47.4 49.7 ug/Kg 105 65-130 <br /> Hexachlorobutadiene ND F1 47.4 27.4 ug/Kg 58 58-132 <br /> 2-Hexanone ND 237 194 ug/Kg 82 44-150 <br /> Isopropylbenzene ND 47.4 46.5 ug/Kg 98 65-130 <br /> 4-Isopropyltoluene ND 47.4 50.7 ug/Kg 107 69-134 <br /> Methylene Chloride ND 47.4 53.1 ug/Kg 112 63.130 <br /> 4-Methyl-2-pentanone(MIRK) ND 237 257 ug/Kg 108 51-140 <br /> Naphthalene ND 47.4 44.8 ug/Kg 94 45-146 <br /> N-Propylbenzene ND 47.4 57.1 ug/Kg 120 70-130 <br /> Styrene ND 47.4 50.9 ug/Kg 107 58.135 <br /> 1,1,1,2-Tetrachloroethane ND 47.4 57.1 ug/Kg 120 64.133 <br /> 1,1,2,2-Tetrachloroethane ND F1 47.4 72.2 F1 ug/Kg 152 70-131 <br /> Tetrachloroethene ND 47.4 47.1 ug/Kg 99 67-130 <br /> Toluene ND 47.4 53.2 ug/Kg 112 70-130 <br /> 1,2,3-Trichlorobenzene ND 47.4 34.8 ug/Kg 73 58.138 <br /> 1,2,4-Trichlorobenzene ND 47.4 37.9 ug/Kg 80 49.144 <br /> 1,1,1-Trichloroethane ND 47.4 53.9 ug/Kg 114 57.133 <br /> 1,1,2-Trichloroethane ND 47.4 55.9 ug/Kg 118 68-132 <br /> Trichloroethene ND 47.4 51.1 ug/Kg 108 66.130 <br /> Trichlorofluoromethane ND 47.4 52.6 ug/Kg 111 61-130 <br /> 1,2,3-Trichloropropane ND F1 47.4 75.5 F1 ug/Kg 159 62-150 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 47.4 52.2 ug/Kg 110 52.130 <br /> ne <br /> 1,2,4-Trimethylbenzene ND 47.4 58.5 ug/Kg 123 64-140 <br /> 1,3,5-Trimethylbenzene ND 47.4 58.2 ug/Kg 123 67.134 <br /> Vinyl acetate ND F1 47.4 ND F1 ug/Kg 0 52-150 <br /> Vinyl chloride ND 47.4 60.6 ug/Kg 128 62-130 <br /> m-Xylene&p-Xylene ND 47.4 49.5 ug/Kg 104 70-130 <br /> o-Xylene ND 47.4 50.5 ug/Kg 106 68-130 <br /> Xylenes,Total ND 94.9 100 ug/Kg 105 70-130 <br /> 2,2-Dichloropropane ND 47.4 56.3 ug/Kg 119 63-130 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-8 romofluorobenzene 90 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 107 60-140 <br /> Toluene-d8(Surr) 98 58-140 <br /> Eurofins TestAmerica, Pleasanton <br /> Page 16 of 49 1/8/2020 <br />