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4 M c C a m b, IIA t i c a l <br />"When Quality Counts" <br />Inc . <br />I <br />1534 Willow Pass ttsburg, CA 94565-1701 <br />Toll Free Telephone: (871W-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com <br />Chow Engineering <br />7770 Pardee Lane, Ste. 100 <br />Oakland, CA 94621-3023 <br />Client Project ID: #11R-120;Ca1Water Date Sampled: <br />Stockton Date Received: <br />12/15/11 <br />12/15/11 <br />Client Contact: Reuben Chow Date Extracted: 12/15/11 <br />Client P.O.: Date Analyzed: 12/16/11 <br />Extraction Method: SW5030B <br />Volatile Organics by P&T and GC/MS (Basic Target List)* <br />Analytical Method: SW8260B <br />Work Order: 1112484 <br />Lab ID <br />1112484-002A <br />Client ID <br />5W <br />Matrix <br />Soil <br />Compound <br />Concentration * <br />DF <br />R , i g <br />Compound <br />Concentration * <br />DF <br />Reporting Limit <br />Acetone <br />ND <br />1.0 <br />0.05 <br />tert-Am 1 methyl ether TAME <br />ND <br />1.0 <br />0.005 <br />Benzene <br />ND <br />1.0 <br />0.005 <br />Bromobenzene <br />ND <br />1.0 <br />0.005 <br />Bromochloromethane <br />ND <br />1.0 <br />0.005 <br />Bromodichloromethane <br />ND <br />1.0 <br />0.005 <br />Bromoform <br />ND <br />1.0 <br />0.005 <br />Bromomethane <br />ND <br />1.0 <br />0.005 <br />2-Butanone MEK <br />ND <br />1.0 <br />0.02 <br />t -Butyl alcohol TBA <br />ND <br />1.0 <br />0.05 <br />n -Butyl benzene <br />ND <br />1.0 <br />0.005 <br />see -Butyl benzene <br />ND <br />1.0 <br />0.005 <br />tert-Butyl benzene <br />ND <br />1.0 <br />0.005 <br />Carbon Disulfide <br />ND <br />1.0 <br />0.005 <br />Carbon Tetrachloride <br />ND <br />1.0 <br />0.005 <br />Chlorobenzene <br />ND <br />1.0 <br />0.005 <br />Chloroethane <br />ND <br />1.0 <br />0.005.1 <br />Chloroform <br />ND <br />1.0 <br />0.005 <br />Chloromethane <br />ND <br />1.0 <br />0.005 <br />2-Chlorotoluene <br />ND <br />1.0 <br />0.005 <br />4-Chlorotoluene <br />ND _1.0___) <br />0.005 I <br />Dibromochlorometh_ane <br />( ND <br />1.0 <br />0.005 <br />1 2-Dibromo-3-chloro ro ane <br />ND <br />1.0 <br />0.004 <br />1 2-Dibromoethane EDB <br />ND <br />I.0 <br />0.004 <br />Dibromometh_ane <br />�ND <br />1.0 <br />_ 0.005 1 <br />1,2 -Dichlorobenzene .. <br />1 ND 1___I <br />0 <br />0,005 <br />13 -Dichlorobenzene <br />ND <br />1.0 <br />0.005 <br />14 -Dichlorobenzene <br />ND 1 <br />1.0 <br />0.005 <br />Dichlorodifluoromethane <br />ND <br />1.0 <br />0.005 <br />1 1-Dichloroethane <br />ND 1 <br />1.0 <br />0.005 <br />H 2-Dichloroethane (1,2 -DCA) <br />ND <br />1.0 <br />0.004 <br />1 1-Dichloroethene <br />ND 1 <br />1.0 <br />0.005 <br />cis-l2-Dichloroethene <br />ND <br />1.0 <br />0.005 <br />trans-l2-Dichloroethene <br />ND 1 <br />1.0 <br />0.005 <br />1 2-Dichloro ro ane <br />ND <br />1.0 <br />0.005 <br />1 3-Dichloro ro ane <br />ND 1 <br />1.0 <br />0.005 <br />2 2-Dichloro ro ane <br />ND <br />1.0 <br />0.005 <br />I 1-Dichloro ro ene <br />ND <br />1.0 <br />0.005 <br />cis - H 3-Dichloro ro ene <br />ND <br />1.0 <br />0.005 <br />trans -1 3-Dichloro ro ene <br />ND <br />1.0 <br />0.005 <br />Diiso ro lether DIPE <br />ND <br />1.0 <br />0.005 <br />Eth lbenzene <br />ND <br />1.0 <br />0.005 <br />Ethyl tert-butyl ether ETBE <br />ND <br />1.0 <br />0.005 <br />Freon 113 <br />ND <br />1.0 <br />0.1 <br />Hexachlorobutadiene <br />ND <br />1.0 <br />0.005 <br />Hexachloroethane <br />ND <br />1.0 <br />0.005 <br />2-Hexanone <br />ND <br />1.0 <br />0.005 <br />Isopropylbenzene <br />ND <br />1.0 <br />0.005 <br />4 -Isopropyl toluene <br />ND <br />1.0 <br />0.005 <br />Meth 1-t-bu t ether MTBE <br />ND <br />1.0 <br />0.005 <br />Methylene chloride <br />ND <br />1.0 <br />0.005 <br />4 -Meth l-2- entanone MIBK <br />ND <br />1.0 <br />0.005 <br />Naphthalene <br />ND <br />1.0 <br />0.005 <br />n -Propyl benzene <br />ND <br />1.0 <br />0.005 <br />S rene <br />ND <br />1.0 <br />0.005 <br />1 1,1,2 -Tetrachloroethane ___I_ <br />ND <br />1.0 ____0.005 <br />1 1,2,2 -Tetrachloroethane <br />ND <br />1.0 <br />0.005 <br />Tetrachloroethene <br />ND <br />1.0 <br />0.005 <br />Toluene <br />( ND <br />1.0 <br />(_.0.005 11,2,3-Trichlorobenzene <br />ND <br />1.0 <br />0.005 <br />1 2 4-Trichlorobenzene <br />ND <br />1.0 <br />0.005 <br />1 1 1 -Trichloroethane <br />ND <br />1.0 <br />0.005 <br />1 1,2 -Trichloroethane <br />ND 1.0 <br />0.005 I <br />Trichloroethene <br />ND <br />1.0 <br />0.005 <br />Trichlorofluoromethane <br />ND <br />1.0 <br />0.005 <br />1 2 3-Trichloro ro ane <br />ND <br />1.0 <br />0.005 <br />1 2 4-Trimeth lbenzene <br />ND <br />1.0 <br />0.005 <br />1 3 5-Trimeth lbenzene <br />ND <br />1.0 <br />0.005 <br />Vial Chloride <br />ND <br />1.0 <br />0.005 <br />Xylenes, Total <br />ND <br />1.0 <br />0.005 <br />Surrogate Recoveries (%) <br />%SS 1: <br />104 <br />1 <br />%SS2: <br />117 <br />%SS3: <br />111 <br />Comments: <br />* water and vapor samples are reported in gg/L, soil/sludge/solid samples in mg/kg, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are <br />reported in mg/L, wipe samples in µg/wipe. <br />ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis; %SS = Percent Recovery of Surrogate <br />Standard; DF = Dilution Factor <br /># surrogate diluted out of range or coelutes with another peak; &) low surrogate due to matrix interference. <br />DHS ELAP Certification 1644 _ Angela Rydelius, Lab Manager <br />Page 9 of 21 <br />