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+ <br />4 M C C a m b e I l A I i C a I <br />"When Quality Counts" <br />Inc . <br />I <br />1534 Will Pass R sburg, CA 94565-1701 <br />Toll Free Telephone: (87 -9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccam)bell.com <br />Chow Engineering <br />7770 Pardee Lane, Ste. 100 <br />Oakland, CA 94621-3023 <br />Client Project ID: #11R-120;CalWater Date Sampled: <br />Stockton Date Received: <br />12/15/11 <br />12/15/11 <br />Client Contact: Reuben Chow Date Extracted: 12/15/11 <br />Client P.O.: Date Analyzed: 12/16/11 <br />Volatile Organics by P&T and GUMS (Basic Target List)* <br />Extraction Method: SW5030B Analytical Method: SW8260B <br />Work Order. 1112484 <br />Lab ID <br />1112484-003A <br />Client ID <br />6E <br />Matrix <br />Soil <br />Compound Concentration * <br />DF <br />Reporting <br />Limit <br />Compound Concentration * DF <br />Reporting <br />Limit <br />Acetone ND <br />1.0 <br />0.05 <br />tert-Am 1 methyl ether JAME <br />ND <br />1.0 <br />0.005 <br />Benzene ND <br />1.0 <br />0.005 <br />Bromobenzene <br />ND <br />1.0 <br />0.005 <br />Bromochloromethane ND <br />1.0 <br />0.005 <br />Bromodichloromethane <br />ND <br />1.0 <br />0.005 <br />Bromoform ND <br />1.0 <br />0.005 <br />Bromomethane <br />ND <br />1.0 <br />0.005 <br />2-Butanone MEK ND <br />1.0 <br />0.02 <br />t -Butyl alcohol TBA <br />ND <br />1.0 <br />0.05 <br />n -Bu 1 benzene ND <br />1.0 <br />0.005 <br />see -Butyl benzene <br />ND <br />1.0 <br />0.005 <br />tert-Butyl benzene ND <br />1.0 <br />0.005 <br />Carbon Disulfide <br />ND <br />1.0 <br />0.005 <br />Carbon Tetrachloride ND <br />1.0 <br />0.005 <br />Chlorobenzene <br />ND <br />1.0 <br />0.005 <br />Chloroethane ND <br />1.0 <br />0.005 <br />Chloroform <br />ND <br />1.0 <br />0.005 <br />Chloromethane ND <br />1.0 <br />0.005 <br />2-Chlorotoluene <br />ND <br />1.0 <br />0.005 <br />4-Chlorotoluene - _ 1 _ ND <br />1.0 <br />0.005 I <br />Dibromochloromethane _ _ _ _-1 <br />ND <br />1.0 0.005 _ <br />1 2-Dibromo-3-chloro ro ane ND <br />1.0 <br />0.004 <br />1 2-Dibromoethane EDB <br />ND <br />1.0 <br />0.004 <br />Dibromomethane_ ND I. <br />1,3 -Dichlorobenzene ND 1 <br />.0__ <br />1.0 <br />0.005_1 _12-Dichlorobenzene <br />0.005 11,4 -Dichlorobenzene <br />ND <br />ND <br />1.0 10.005 <br />1.0 0.005 <br />Dichlorodifluoromethane ND <br />1.0 <br />0.005 <br />11-Dichloroethane <br />ND <br />1.0 <br />0.005 <br />] 2-Dichloroethane 12 -DCA ND <br />1.0 <br />0.004 <br />1 1-Dichloroethene <br />ND <br />1.0 <br />0.005 <br />cis -1 2-Dichloroethene ND <br />1.0 <br />0.005 <br />trans -1 2-Dichloroethene <br />ND <br />1.0 <br />0.005 <br />] 2-Dichloro ro ane ND <br />1.0 <br />0.005 <br />1 3-Dichloro ro ane <br />ND <br />1.0 <br />0.005 <br />2 2-Dichloro ro ane ND <br />1.0 <br />0.005 <br />1 1-Dichloro ro ene <br />ND <br />1.0 <br />0.005 <br />cis -1 3-Dichloro ro ene ND <br />1.0 <br />0.005 <br />trans -1 3-Dichloro ro ene <br />ND <br />1.0 <br />0.005 <br />Diiso ro 1 ether DIPE ND <br />1.0 <br />0.005 <br />Eth (benzene <br />ND <br />1.0 <br />0.005 <br />Ethyl tert-butyl ether ETBE ND <br />1.0 <br />0.005 <br />Freon 113 <br />ND <br />1.0 <br />0.1 <br />Hexachlorobutadiene ND <br />1.0 <br />0.005 <br />Hexachloroethane <br />ND <br />1.0 <br />0.005 <br />2-Hexanone ND <br />1.0 <br />0.005 <br />Isopropylbenzene <br />ND <br />1.0 <br />0.005 <br />4-1sopropyl toluene ND 1 <br />1.0 <br />0.005 <br />Meth I-t-bu 1 ether MTBE <br />ND <br />1.0 <br />0.005 <br />Methylene chloride ND <br />1.0 <br />0.005 <br />4 -Meth I-2- entanone MIBK <br />ND <br />1.0 <br />0.005 <br />Naphthalene ND <br />1.0 <br />0.005 <br />n -Propyl benzene <br />ND <br />1.0 <br />0.005 <br />Styrene _ ND <br />I.0 <br />_j 0.005_L <br />l,l 12 -Tetrachloroethane_ <br />_ ND <br />( 1.0 _1 <br />0.005 <br />1 1 2 2 -Tetrachloroethane ND <br />1.0 <br />0.005 <br />Tetrachloroethene <br />ND <br />1.0 <br />0.005 <br />Toluene ND <br />1.0 <br />0.005 ( <br />1,2,3-Trichlorobenzene <br />ND <br />1.0 <br />0.005 <br />1 2 4-Trichlorobenzene ND <br />1.0 <br />1 0.005 <br />1J, 1 -Trichloroethane <br />ND <br />1.0 <br />0.005 <br />1 1,2-Trichloroethane1_ ND j <br />1.0 <br />0.005 I <br />Trichloroethene _ _ _ <br />ND <br />I.0 _LO _ <br />Trichlorofluoromethane ND <br />1.0 <br />0.005 <br />1 2 3-Trichloro ro ane <br />ND <br />1.0 <br />0.005 <br />12 4-Trimeth (benzene ND <br />1.0 <br />0.005 <br />] 3 5-Trimeth (benzene <br />ND <br />1.0 <br />0.005 <br />Vinyl Chloride ND <br />1.0 <br />i 0.005 <br />Xylenes, Total <br />ND <br />1.0 <br />0.005 <br />Surrogate Recoveries (%) <br />%SSI : <br />105 <br />%SS2: <br />116 <br />%SS3: <br />112 <br />Comments: <br />* water and vapor samples are reported in pg/L, soil/sludge/solid samples in mg/kg, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are <br />reported in mg/L, wipe samples in pg/wipe. <br />ND means not detected above the reporting limit/method detection limit, N/A means analyte not applicable to this analysis; %SS = Percent Recovery of Surrogate <br />Standard; DF = Dilution Factor <br /># surrogate diluted out of range or coelutes with another peak, &) low surrogate due to matrix interference. <br />DHS FLAP Certification 1644 _ Angela Rydelius, Lab Manager <br />Page 10 of 21 <br />