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WORLD OIL RECYCLING ICP P , E 5300 DV QA REPORT FORM DATE : 4/27/2018 ANALYST: 12P ANALYTE ICV % REC . ICS ICSA % REC , ICSAB MREC LOS . CCV % REC CCB <25 518 104 478 1010 101 <25 Pb 1013 101 <'25 Cu 1022 102 <25 406 99 452 1030 103<25 498 100 473 1000 100 <25 Zn 1006 101 <25 TI 1005 101 <25 508 102 476 995 100 <25 Asff9899 <25 504 101 498100 101 51 984 98<25 500100 482 96 110 55 1032 103 <26 Cr102 < 5 NI102 < 25 487 97 465 93 106 53 1022 102<25 - 507 101 488 98 97 49 1002 100 <25 Cd100 r28 Ag 1032 '103 <25 503 101 489 98 101 51 1045 105 <25 Be 1036 104 <25 t5004 101 484 97 102 51 1046 105 <25 Se 993 99 <25 100 490 98101 51 976 98 <25 Be 1007 101 <25 101 489 98 102 51 1008 101 <25 Mo 993 99 <25 513 103 503 101 102 51 998 100 < 25 498 100 488 98 101 51 977 98 <25 5b 969 9Z <25 V 1020 102_ <25 494 99 500 100 99 50 1027 103 <25 512 102 453 91 100 50 1007 101 <25 Co 1001 100 <25 Sn 981 98 <25 503 101 483 97 100 50 983 98 ANALYTE CCV % REG, GCE CCV % REC , CCB CCV °h REC , CCB CCV % REG, CCB Pb 1014 101 <25 996 100 <25 Cu 1027 103 <25 1020 102 <25 Zn 997 100 <25 987 99 <25 TI 1000 100 <25 984 98 <25 As 990 99 <25 973 97 <25 Cr 1029 103 <25 1021 102 _ <25 Ni 1024 102 <25 1008 101 <25 _ Cb 1003 100 <25 988 99 <25 Ay 1043 104 <25 1033 103 <25 Ba 1046 105 <25 1037 104g<� 2Se 976 98 <25 959 96 Be 1004 100 <25 997 100Mo 1003 100 <25 987 99 Sb 979 98 <25 959 96 <25 V 1027 103 <26 1015 102 <25 Co 1010 101 <25 993 99 <25 Sn 989 99 <25 976 98 <25 ICV. - INITIAL CALIBRATION VERIFICATION ICSA, - INTERFERENT CHECK STANDARD SOLUTION 0, 5 PPM CCV, - CONTINUING CALIBRATION VERIFICATION fCSAB, - INTERFERENT CHECK STANDARD SOLUTION 0. 5 PPM ICB . • INITIAL CALIBRATION BLANK % R CRITERIA ON ICSA 80420 CCB. - CONTINUING CALIBRATION BLANK % R CRITERIA ON ICSAB 80. 120 % CRITERIA ON ICV 900110 LCs- LABORATORY CONTROL SAMPLE % CRITERIA ON CCV 80420 %R CRITERIA ON LOS 85415 DATE: ): CHECKED BY > �} ' �3. 1 6 rte, [?ATL"' REVIEWED BY : ,_ .