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CERTIFICATE NUMBER: 1573 <br />EXPIRATION DATE: 7/31/95 <br />10.13 <br />Selenium <br />7740(06.06.86) _____________________ <br />Y <br />10.19 <br />Cyanide <br />7741(-------- )-----------•••------- <br />N <br />9010(06-06-86)------------------------- <br />Y <br />10.14 <br />Silver <br />10.20 <br />Fluoride <br />7760(06-06.86)_____________________ <br />Y <br />300.0(11-30-93)------------------------ <br />Y <br />7761(--------)--------------------- <br />N <br />340.1(-------- )------------------------ <br />N <br />10.15 <br />Thaliius <br />340.2(06-06-86)------------------------ <br />Y <br />(-------- ) ----------------•---- <br />N <br />340.3(-------- ) ------------------------ <br />N <br />7841(06-06-86)--•----------••------ <br />T <br />10.21 <br />Sulfide <br />10.16 <br />vanadium <br />(06-06-86)------------------------- <br />Y <br />7910(-------- )----•---------------- <br />N <br />10.22 <br />Total Organic Lead <br />7911(-------- ) --------------------- <br />N <br />(........ ) ............................. <br />N <br />10.17 <br />Zine <br />10.23 <br />EPA Method 6010(06-06-86)------------•- <br />Y <br />7450(06-06-86)---•----•--------•--- <br />Y <br />10.24 <br />EPA Method 6020111-30.93)-------------- <br />y <br />10.18 <br />1(...--...)--------------------- <br />Chromium (VI) <br />N <br />7195(........)--------------------- <br />N <br />i <br />7196(06-06-86)-------•------------- <br />Y <br />7197(...-----)---•----------------- <br />N <br />7198(.-------) --------------------- <br />N <br />11 <br />ExtracUM Isola of Nara Waste <br />(06-06-86) <br />11.1 <br />California Waste Extraction Test (YET) (Title 22, <br />CCR. 66261.100, Appendix II) ------------------- <br />Y <br />11.2 <br />Extraction Procedure Toxicity•----•-------------------------------------------------------------- <br />Y <br />11.3 <br />Toxicity Characteristic Leaching Procedure (TCLP) <br />All Classes----------------------------------- <br />Y <br />11.4 <br />Toxicity Characteristic Leaching Procedure (TCLP) <br />inorganics <br />Only ----•--------------------------- <br />N <br />11.5 <br />Toxicity Characteristic Leaching Procedure (TCLP) <br />Extractable* Only ------------------------------ <br />N <br />11.6 <br />Toxicity Characteristic Leaching Procedure (TCLP) <br />Volatiles Only --------------------------------- <br />N <br />12 <br />12.1 <br />Organic Ch istly of NazatSkM Waste <br />( <br />by Gcros <br />coabinatien) <br />Method 8240(02-05.87) <br />EPA ..................................................................•----- <br />Y <br />12.2 <br />EPA Method 0(-----•--)........................................................................ <br />N <br />12.3 <br />EPA method (02-05.87)-----------.------------------------------------•--- <br />--------------•-- <br />Y <br />12.4 <br />EPA Method 8280(.-------)........................................................................ <br />N <br />12.5 <br />EPA Method 8290( -------- -------------------------------•-•------__----------------•------------- <br />N <br />12.6 <br />EPA Method (11-30-93)------------------------------------------------------------------------ <br />Y <br />13 <br />Ommir. Manistm 2f."armakm Waste <br />(exciudim <br />is by GC/Ms c9onation) <br />] <br />! <br />13.1 <br />EPA Method 8010(-------•) •------••- <br />N <br />13.13 <br />EPA Method 8310(05-27-92)-------------- <br />Y <br />13.2 <br />EPA Method 8015(01-09-90)----•----- <br />Y <br />13.14 <br />EPA Method 632 (07-15-91)-------------- <br />Y <br />13.3 <br />EPA Method 8020(06.06-86) .......... <br />Y <br />13.15 <br />Total Petroleum Hydrocarbons <br />13.4 <br />EPA Method 8030(--------)--•------• <br />N <br />(LOFT Manual) (06-06-96) --------------- <br />Y <br />13.5 <br />EPA Method 8040(------•-) ---------- <br />N <br />13.16 <br />EPA Method 8011(11-08-87)-------------- <br />Y <br />13.6 <br />EPA Method 8060(--------)--------•- <br />N <br />13.17 <br />EPA Method 8021( -------- •-•---•------- <br />N <br />13.7 <br />EPA Method 8080(06-06.86)-------•-- <br />Y <br />13.18 <br />EPA Method 8070(--------) .............. <br />N <br />13.8 <br />EPA Method 8040(--------)---------- <br />N <br />13.19 <br />EPA Method 8110(---.----) <br />N <br />13.9 <br />EPA Method 8100(-------- )---------- <br />N <br />13.20 <br />EPA Method 8141(11-30.93) ----•--•------ <br />Y <br />13.10 <br />EPA Method 8120(--------)--------•- <br />N <br />13.21 <br />EPA Method 8330(--------)-------------- <br />N <br />13.11 <br />EPA Method 8140(06-06-86)----•----- <br />Y <br />13.12 <br />EPA Method 8150(06-06.86)---------- <br />Y <br />14 <br />Bulk Asbestos Ansivsis (--------) <br />J <br />14.1 <br />1% or Greater Asbestos Concentrations (Title 22, <br />CCR, 66261.24(a)(2)(A))--------------------------N <br />15 <br />Substances Regulated i1aft the California Safe Drinking Water <br />and U-Mc-Enforcement To-Mc-EnforcementAct (Proposition <br />65) and Not InctUft in Otherlisted <br />G <br />16 <br />Wastarater IMMMig Chemistry. Nutrients and Demand (07-15-91) <br />16.1 <br />Acidity---------------------------- <br />Y <br />16.12 <br />Cyanide-------------------------------- <br />Y <br />16.2 <br />Alkalinity-----•-•-----------•----- <br />y <br />16.13 <br />Cyanide amenable to Chlorination------- <br />Y <br />- <br />16.3 <br />Ammonia ---------------------------- <br />y <br />16.14 <br />Fluoride-•-----•----------------------- <br />Y <br />16.4 <br />16.5 <br />Biochemical oxygen Omand .......... <br />Boron •----------------------------- <br />Y <br />Y <br />16.15 <br />16.16 <br />Hardness-----•------------------------- <br />Kjeldahl Nitrogen <br />Y <br />16.6 <br />Bromide------•--------------------- <br />Y <br />16.17 <br />---------------------- <br />Magnesium------------------------------ <br />Y <br />Y <br />16.7 <br />Calcium •----•---------------------- <br />Y <br />16.18 <br />Nitrate-------------------------------- <br />Y <br />16.8 <br />cBOD------------------------------- <br />N <br />16.19 <br />Nitrite-------------------------------- <br />Y <br />16.9 <br />Chemical Oxygen o------------- <br />y <br />16.20 <br />oil and Grease------------------------- <br />Y <br />16.10 <br />Chloride--------------------------- <br />Y <br />16.21 <br />Organic Carbon ------------------------- <br />Y <br />16.11 <br />Chlorine Residual, total----------- <br />y <br />16.22 <br />oxygen, Dissolved ------------•--•-- ---- <br />Y <br />Page -3- <br />