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Page -4- CERTIFICATE NUMBER: 1573 EXPIRATION DATE: 7/31/95 16.23 PH Y 16.39 Surfactants (MBAS) -------------------- Y 16.24 Phenols ----•------ Y 16.40 Tannin and Lignin --------------------- Y 16.25 Phosphate, Ortho- -------•---------- Y 16.41 Turbidity ---•------------------------- Y 16.26 Phosphorus, total ---------------•-- Y 16.42 Iran (Colorimetric Only) -------------- N 16.27 Potassium ------------•---•-------•- Y 16.43 Manganese (Colorimetric Only) --------- N 16.28 Residue, Total --------------------- Y 16.44 Total Recoverable 16.29 Residue Filterable (TOS) Y Petroleum Hydrocarbons •--------------- Y 16.30 Residue, Nonfitteroble (TSS) ------- Y 16.45 Total organic Halides ----------------- Y 16.31 Residue, Settleable (SS) ----------- Y 16.32 Residue, Volatile --------•--------- Y 16.33 Silica -••--------------------•----- Y 16.34 Sodium ----------------------------- Y 16.35 Specific Conductance ---•-••---•-•-- Y 16.36 Sulfate ---------------------------- Y 16.37 Sulfide (includes total 3 soluble) - Y 16.38 Sulfite --•••--••---•--------------- Y 17 Toxic Chemical Elements in wastewater (07-15-91) 17.1 Aluminum ........................... Y 17.18 Nickel -----•----•-------------------- Y 17.2 Anti ----•-------•-------------- Y 17.19 Osmium --- ............. N 17.3 Arsenic ------•------•-----•---•-•-- Y 17.20 Palladium -•_________________•........ N 17.4 Barium -------------•------••------ Y 17.21 Platinum --- ------------ N 17.5 Beryllium -------------------•------ Y 17.22 Rhodium ------------------------------ N 17.6 Cadmium •-------•------------------- Y 17.23 Ruthenium ---------------------------- N 17.7 Chromium (VI) ---------------------- Y 17.24 Selenium -------------------------•--- Y 17.8 Chromium, total ---------•---------- Y 17.25 Silver -----••------------------------ Y - 17.9 Cobalt ---------•------------------- Y 17.26 Strontium Y 17.10 Copper ------------------------•---- Y 17.27 Thallium ----------------------------- Y 17.11 Gold ------------------------------- Y 17.28 Tin ---------------------------------- Y 17.12 Iridium ---------•--------------••-- N 17.29 Titanium ----•------------------------ Y 17.13 Iron •------------------------------ Y 17.30 Vanadium ----------------------------- Y 17.14 Lead ••--••------------------------- Y 17.31 Zinc --------------------------------- Y 17.15 Manganese ------••-•----------•----- Y 17.32 EPA Method 200.7 --------------------- Y 17.16 Mercury --------•----•-------------- Y 17.33 EPA Method 200.8 ----•---------------- Y 17.17 Mol •------------------------ Y 17.34 OCP ---------------------------------- N 17.35 Asbestos •-------•-------------------- N 18 OtMic Chemistry of wastewater ( s by GC/MS combination (07-15-91) r 18.1 EPA Method 624-----•-----------------•-.--..-...-..-...--._-_--•.---..-.-..-..----------.------- Y E18.2 EPA Method 625--------------------------------------------•---•-----.--------------..__..------- Y 18.3 EPA Method 1613--------------------------------------------------------------------•------------ N 18.4 EPA Method 1625--------------------------------------------------------------------------------- N 18.5 EPA Method 613•--•-----------------------------•.-.-------..-...-------------------------------- N 19 Organic Cheaistrr of wastewater (excludi!q Seemawments by GC/MS combination) (07-15-91) 19.1 EPA Method 601 ----•---------------• N 19.8 EPA Method 608 --------------•-------- Y 19.2 EPA Method 602 --•-----••----------- Y 19.9 EPA Method 609 --•--•----------------- N 19.3 EPA Method 603 -•------------------- N 19.10 EPA Method 610 ----------------------- Y 19.4 EPA Method 604 ------•-•------------ N 19.11 EPA Method 611 ----------------------- N 19.5 EPA Method 605 -•-----------•------- N 19.12 EPA Method 632 ----------------------- Y 19.6 EPA Method 606 •-------------------- N 19.13 EPA Method 619 --•-------------------- N 19.7 EPA Method 607 ------------•---•---- N 19.99 EPA Method 615 ----------------------- Y 20 Inereanic Chmistry and Toxic Chmical gtgEM of Pesticide Resighm in Food (--------) 20.1 Processed Foods by One of the Following Methods Atomic Absorption Spectrophotometry------------------------------------------------------- N Inductively Coupled Plasma Atomic Emission Spectrophotometry ---------- ................... N Inductively Coupled Ptasms/Mass Spectrometry ---------------------------------------------- N Colorimetry---.-----•--------------------------------------------------------------------- N 20.2 Raw Commodities by One of the Following Methods Atomic Absorption Spectrophotometry ---•-•----------•-•----------------•-•---------•------- N Inductively Coupled K8880 Atomic Emission Spectrophotometry -------•---------------------- N Inductively Coupled Ptasma/Mass Spectrometry ---------------------------------------------- N Colorimetric------------------------------------------------------------ --- N 20.3 Dairy Products by one of the Following Methods Atomic Absorption Spectrophotometry....................................................... N Inductively Coupled Plasma Atomic Emission Spectrophotometry ------------------------------ N Inductively Coupled Plasms/Mass Spectrometry ---------------------------------------------- N Colorimetry-------------------------------------•_..----•---_-----_..._-_-_--__-_-_-_..___ N Page -4-