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819 Striker Ave Ste 8 <br /> 834 <br /> Sequoia Sam(916)9nto.C21-99600 <br /> Analytical FAXequoi labsx00 <br /> www.segtwialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County S310191 <br /> 1326 N.Market Blvd, Project Number: 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100237-EPA 5030B[P/TJ <br /> Blank(3100237 BLKI) Prepared: 10/16/03 Analyzed: 10/17/03 <br /> Trichlorofluoromethane ND 0.42 0.50 ug/1 <br /> 1,2,3-Trichloropropane ND 0.55 1.0 <br /> 1,2,4-Trimethylbenzene ND 0.18 0.50 <br /> 1,3,5-Trimethylbenzene ND 0.28 0.50 " <br /> Vinyl chloride ND 0.16 0.50 <br /> Xylenes(total) ND 0.48 0.50 <br /> Surrogate:DibromoJluoromethane 10.3 10.0 103 70-130 <br /> Surrogate:1,2-DCA-d4 11.2 10.0 112 70-130 <br /> Surrogate:Toluene-d8 9.97 10.0 100 70-130 <br /> Surrogate:4-BFB 8.89 10.0 89 70-130 <br /> Laboratory Control Sample(3100237-BSI) Prepared&Analyzed: In/16/03 <br /> Benzene 25.6 0.28 0.50 ug/l 25.0 102 70-130 <br /> Chlorobenzene 25.3 0.32 0.50 25.0 101 70-130 <br /> 1,1-Dichloroethene 26.9 0.24 0.50 25.0 108 70-130 <br /> Toluene 25.8 0.32 0.50 " 25.0 103 70-130 <br /> Trichloroethene 19.4 0.36 0.50 25.0 78 70-130 <br /> Surrogate:DibromoJluoromethane 25.3 25.0 101 70-130 <br /> Surrogate:1,2-DCA-d4 25.5 i 25.0 102 70-130 <br /> Surrogate:Toluene-d8 25.3 25.0 101 70-130 <br /> Surrogate:4-BFB 25.2 25.0 101 70-130 <br /> Matrix Spike(3100237 MSI) Source:5310197-06 Prepared: 10/16/03 Analyzed: 10/17/03 <br /> Benzene 23.5 0.28 0.50 ug/l 25.0 ND 94 60-140 <br /> Chlorobenzene 24.8 0.32 0.50 25.0 ND 99 60-140 <br /> 1,1-Dichloroethene 26.3 0.24 0.50 25.0 ND 105 60-140 <br /> Toluene 25.3 0.32 0.50 „ 25.0 ND 101 60-140 <br /> Trichloroethene 18.8 0.36 0.50 25.0 ND 75 60-140 <br /> Surrogate:DibromoJluoromethane 23.4 25.0 94 70-130 <br /> Surrogate:1,2-DCA-d4 24.9 25.0 100 70-130 <br /> Surrogate:Toluene-d8 25.2 25.0 101 70-130 <br /> Surrogate:4-BFB 25.7 25.0 103 70-130 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance With the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 50 of 66 <br />