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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> A (916)921-9600 <br /> A <br /> ' nalytical FAX(916)921-0100 <br /> www.sequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County 5310191 <br /> 1326 N.Market Blvd. Project Number. 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> ' Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100237-EPA 5030B IP/T] <br /> Matrix Spike Dup(3100237-MSD1) Source:5310197-06 Prepared: 10/16/03 Analyzed: 10/17/03 <br /> ' Benzene 23.3 0.28 0.50 ug/l 25.0 ND 93 60-140 0.9 25 <br /> Chlorobenzene 24.3 0.32 0.50 25.0 ND 97 60-140 2 25 <br /> I,1-Dichloroethene 25.6 0.24 0.50 25.0 ND 102 60-140 3 25 <br /> Toluene 24.8 0.32 0.50 25.0 ND 99 60-140 2 25 <br /> Trichloroethene 18.0 0.36 0.50 25.0 ND 72 60-140 4 25 <br /> Surrogate:Dibromofluoromethane 24.1 25.0 96 70-130 <br /> Surrogate:1,2-DCA-d4 25.3 25.0 101 70-130 <br /> Surrogate:Toluene-d8 25.5 25.0 102 70-130 <br /> Surrogate:4-BFB 24.8 25.0 99 70-130 <br /> Batch 3100255-EPA 5030B [P/TI <br /> Blank(3100255-BLKI) Prepared&Analyzed: 10/17/03 <br /> 2-Butanone ND 0.14 0.50 ug/l <br /> 2-Chloroethylvinyl ether ND 0.22 0.50 " <br /> 2-Hexanone ND 0.26 0.50 <br /> 4-Methyl-2-pentanone ND 0.17 0.50 <br /> Acetone 1.04 0.52 2.0 J <br /> Acetonitrile ND 2.4 5.0 " <br /> Acrolein ND 0.70 5.0 <br /> Acrylonitrile ND 0.26 2.0 <br /> Allyl chloride ND 0.14 0.50 " <br /> ' Carbon disulfide ND 0.29 0.50 „ <br /> Chloroprene ND 0.10 0.50 <br /> cis-1,3-Dichloropropene ND 0.11 0.50 <br /> Freon 113 ND 0.25 0.50 " <br /> ' Iodomethane ND 0.036 0.50 <br /> Isobutanol ND 0.61 5.0 <br /> m,p-Xylene ND 0.38 0.50 " <br /> ' Methacrylonitrile ND 0.73 1.0 <br /> Methyl methacrylate ND 0.20 0.50 <br /> o-Xylene ND 0.15 0.50 <br /> Propionitrile ND 2.7 5.0 " <br /> ' trans-1,3-Dichloropropene ND 0.10 0.50 <br /> trans-1,4-Dichloro-2-butene ND 0.42 0.50 <br /> Vinyl acetate ND 0.94 2.0 " <br /> ' Benzene ND 0.28 0.50 " <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 51 of 66 <br />