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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916)921-9600 <br /> qAW FAX92oOAnalytical wwwsequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San JoaquinCounty Coun S310191 <br /> 1326 N.Market Blvd. Project Number: 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Semivolatile Organic Compounds by EPA Method 8270C - Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result NIDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100205-EPA 3510C Sep Funnel <br /> Blank(3100205-BLKl) Prepared: 10/15/03 Analyzed: 10/21/03 <br /> 2,4-Dinitrophenol ND 6.4 20 ug/1 <br /> 4-Nitrophenol ND 3.7 20 <br /> Dibenzofuran ND 2.6 5.0 <br /> 2,4-Dinitrotoluene ND 2.9 5.0 " <br /> Diethyl phthalate ND 2.3 5.0 ; <br /> 4-Chlorophenyl phenyl ether ND 2.1 5.0 <br /> Fluorene ND 22 5.0 <br /> 4,6-Dinitro-2-methylphenol ND 4.5 20 " <br /> N-Nitrosodiphenylamine ND 3.1 5.0 " <br /> Azobenzene ND 2.8 5.0 <br /> 4-Nitroaniline ND 3.3 5.0 " <br /> 4-Bromophenyl phenyl ether ND 2.4 5.0 <br /> Hexachlorobenzene ND 22 5.0 " <br /> Pentachlorophenol ND 4.4 20 " <br /> Phenanthrene ND 2.4 5.0 " <br /> Anthracene ND 25 5.0 <br /> Carbazole ND 32 5.0 <br /> Di-n-butyl phthalate ND 2.7 5.0 " <br /> Fluoranthene ND 2.4 5.0 <br /> Pyrene ND 2.8 5.0 <br /> Benzyl butyl phthalate ND 2.6 5.0 <br /> 3,3'-Dichlorobenzidine ND 8.7 10 " <br /> ' Bis(2-ethylhexyl)phthalate ND 25 5.0 <br /> Benzo(a)anthracene ND 2.4 5.0 <br /> Chrysene ND 2.3 5.0 " <br /> Di-n-octyl phthalate ND 3.0 5.0 " <br /> Benzo(b&k)fluoranthene(total) ND 10 10 <br /> Benzo(a)pyrene ND 2.7 5.0 <br /> Indeno(1,2,3-cd)pyrene ND 42 5.0 " <br /> Dibenz(a,h)anthracene ND 4.6 5.0 <br /> Benzo(ghi)perylene ND 4.5 5.0 <br /> Surrogate:2-Fluorophenol 59.6 150 40 11.2-69.6 <br /> ' Surrogate:Phenol-d6 34.7 II 150 23 70-58.7 <br /> Surrogate:Nitrobenzene-d5 74.4 100 74 36.7-118 <br /> Surrogate:2-Fluorobiphenyl 76.4 100 76 44-112 <br /> Surrogate:2,4,6-Tribromophenol 114 150 76 41.5-117 <br /> ' Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 61 of 66 <br />