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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916)921-9600 <br /> Analytical FAXequoi labs.c00 <br /> www.sequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County S310191 <br /> 1326 N.Market Blvd. Project Number: 791291 /00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Semivolatile Organic Compounds by EPA Method 8270C- Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100205-EPA 3510C Sep Funnel <br /> Blank(3100205 BLKi) Prepared: 10/15/03 Analyzed: 10/21/03 <br /> Surrogate:Terphenyl-d14 91.3 ug/l 100 91 20.7-144 <br /> Laboratory Control Sample(3100205-BS1) Prepared: 10/15/03 Analyzed: 10/21/03 <br /> Phenol 44.0 3.0 5.0 ug/t 150 29 22-117 <br /> 2-Chlorophenol 118 5.3 10 „ 150 79 28-111 <br /> 1,4-Dichlorobenzene 87.3 3.9 5.0 100 87 29-108 <br /> N-Nitrosodi-n-propylamine 91.0 3.8 5.0 100 91 29-119 <br /> 1,2,4-Trichlorobenzene 90.5 3.8 5.0 100 90 24-131 <br /> 4-Chloro-3-methylphenol 130 4.7 5.0 150 87 51-116 <br /> Acenaphthene 93.1 2.7 5.0 100 93 58-120 <br /> 4-Nitrophenol 42.8 3.7 20 150 29 9.57-53.8 <br /> 2,4-Dinitrotoluene 97.3 2.9 5.0 100 97 60-140 <br /> Pentachlorophenol 112 4.4 20 150 75 41.6-103 <br /> Pyrene 119 2.8 5.0 100 119 52-127 <br /> Surrogate:l-Fluorophenol 61.6 150 41 11.2-69.6 <br /> Surrogate:Phenol-d6 39.8 150 27 10-58.7 <br /> Surrogate:Nitrobenzene-d5 74.0 100 74 36.7-118 <br /> Surrogate:2-Fluorobiphenyl 77.6 100 78 44-112 <br /> ' Surrogate:2,4,6-Tribromophenol 137 150 91 41.5-1/7 <br /> Surrogate:Terphenyl-d14 98.7 100 99 20.7-144 <br /> Laboratory Control Sample Dup(3100205-BSD1) Prepared. 10/15/03 Analyzed: 10/21/03 <br /> Phenol 46.2 3.0 5.0 ug/l 150 31 22-117 5 22 <br /> ' 2-Chlorophenol 123 5.3 10 150 82 28-111 4 39 <br /> 1,4-Dichlorobenzene 89.8 3.9 5.0 100 90 29-108 3 41 <br /> N-Nitrosodi-n-propylamine 91.8 3.8 5.0 100 92 29-119 0.9 44 <br /> ' 1,2,4-Trichlorobenzene 92.0 3.8 5.0 100 92 24-131 2 48 <br /> 4-Chloro-3-methylphenol 131 4.7 5.0 150 87 51-116 0.8 30 <br /> Acenaphthene 92.3 2.7 5.0 100 92 58-120 0.9 27 <br /> 4-Nitrophenol 47.8 3.7 20 150 32 9.57-53.8 11 44 <br /> 2,4-Dinitrotoluene 97.1 2.9 5.0 I, 100 97 60-140 0.2 22 <br /> Pentachlorophenol 108 4.4 20 150 72 41.6-103 4 33 <br /> Pyrene 116 2.8 5.0 100 116 52-127 3 25 <br /> ' Surrogate:2-Fluorophenol 65.1 150 43 11.2-69.6 <br /> Surrogate:Phenol-d6 41.6 150 28 10-58.7 <br /> Surrogate:Nitrobenzene-d5 77.0 100 77 36.7-118 <br /> Surrogate:2-Fluorobiphenyl 78.5 100 78 44-112 <br /> ' Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> ' This analytical report must be reproduced in its entirety. <br /> Page 62 of 66 <br />