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Sep 24 2004 10:17AM McCAMPHELL ANALYTICAL 9257984612 <br />p.5 <br />McCampbell Analytical, Inc. <br />4 <br />110 2nd Avenue South, #D7, Pacheco. CA 94553-5560 <br />Telepbow:925-798-1620 Fax:925-798-1622 <br />Website: www.mccanpbell.com E -nail: main@rwcatnpbelt.com <br />Allied Waste <br />1145 West Charter Way <br />Stockton, CA 95206 <br />Diesel (C10-23) and <br />tractionmethod: SW3550C <br />Lab ID Client ID <br />Client Project ID: #926900-1733; FU -04 <br />Date Sampled; 09/16/04 <br />Date Received: 09/21/04 <br />Client Contact: Brad Bonner <br />Date Extracted: 09/21/04 <br />Client P.O.: Date Analyzed: 09/23/04 <br />Oil (C18+) Range Extractable Hydrocarbons with Silica Gel Cleaa-Up* <br />Analytical methods: SW8015C Work Order. 0409325 <br />Matrix TPH(d) TPH(mo) DF % SS <br />0409325-OOIA <br />Comp#1 <br />S <br />4600,gb <br />17,000 <br />100 <br />108 <br />0409325-002A <br />Comp#2 <br />S <br />I1,000,g,b <br />27,000 <br />100 <br />105 <br />Reporting Limit for DF =1; <br />ND means not detected at or <br />above the reporting limit <br />W <br />NA <br />NA <br />ug/L <br />S <br />1.0 <br />5.0 <br />mg/Kg <br />* water samples are reported in pg/L, wipe samples in pg/wipe, soil/solid/sludge samples in mg/kg, productloil/non-aqueous liquid samples in mg/L- <br />and al l DISTLC / STLC / SPLP / TCLP extracts are reported in pg/L, <br /># cluttered chromatogram resulting in cocluted surrogate and sample peaks, or; surrogate peak is on elevated baseline, or; surrogate has been diminished <br />by dilution of original extract. <br />+The following descriptions ofthe TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation: a) <br />unmodified or weakly modified diesel is significant; b) diesel range compounds are significant; no recognizable pattern; e) aged diesel? is significant); <br />d) gasoline range compounds are significant; e) unknown medium boiling point pattern that does not appear to be derived from diesel; f) one to a few <br />isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheentproduct is present; i) liquid sample that contains <br />greater than —1 vol. % sediment; k) kerosene/kerosene range; l) bunker oil; m) fuel oil; n) stoddard solventimineral spirit. <br />DHS Certification No. 1644 j Angela Rydelius, Lab Manager <br />