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McCampbell Analytical, Inc. <br />Z4 <br />110 2nd Avenue South, #D7, Pacheco, CA 94553-5560 <br />Telephone: 925-798-1620 Fax: 925-798-1622 <br />1 Website: www.n=anVbell.com Ismail: main@rmcarMbell.com <br />Allied Waste <br />1145 West Charter Way <br />Stockton, CA 95206 <br />Client Project ID: #916900/1733/4792; <br />STP -FU -4 <br />Date Sampled: 10/06/04 <br />Date Received: 10/07/04 <br />Client Contact: Brad Bonner <br />Date Extracted: 10/07/04 <br />Client P.O.: <br />Date Analyzed: 10/07/04 <br />Diesel Range (C10 -C23) Extractable Hydrocarbons with Silica Gel Clean -Up* <br />xtraction method: SW3550C Analytical methods: SW8015C Work Order. 0410089 <br />Lab ID <br />Client ID <br />Matrix <br />TPH(d) <br />DF <br />% SS <br />0410089-OOIA <br />Comp#1 <br />S <br />3100,g,b <br />200 <br />98.0 <br />0410089-002A <br />Comp#2 <br />S <br />2100,g,b <br />200 <br />88.0 <br />I <br />Reporting Limit for DF =1; W NA NA <br />ND means not detected at or — —d <br />above the reporting limit S 1.0 mg/Kg <br />* water samples are reported in pg/L, wipe samples in gg/wipe, soil/solid/sludge samples in mg/kg, product/oil/non-aqueous liquid samples in mg/L, and <br />all DISTLC / STLC / SPLP / TCLP extracts are reported in pg/L. <br />cluttered chromatogram resulting in coeluted surrogate and sample peaks, or; surrogate peak is on elevated baseline, or; surrogate has been diminished <br />1 dilution of original extract. <br />+The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation: a) <br />unmodified or weakly modified diesel is significant; b) diesel range compounds are significant; no recognizable pattern; c) aged diesel? is significant); d) <br />gasoline range compounds are significant; e) unknown medium boiling point pattern that does not appear to be derived from diesel; f) one to a few <br />isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheen/product is present; i) liquid sample that contains <br />greater than –1 vol. % sediment; k) kerosene/kerosene range; 1) bunker oil; m) fuel oil; n) stoddard solvent/riineral spirit. <br />DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />