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'as little agitation as possible to reduce potential loss of volatile constituents, Major ions, TDS, <br /> and metals analyses Cm non-preserved containers) will be collected <br /> be collected in preserved containernext followed <br /> by samples to <br /> s. Containers will be filled directly from the disposable bailer, <br /> immediately capped,and placed in a temp -monitotrd iced chest. Caution will be used not <br /> to overfill bottles containing a preservative. Temperature will be monitored by placing a <br /> flMmometer in the chest and checlqng to make sure that there is'sufficiccnt ice in the chest to <br /> a tem c of'approximately <br /> . 4 degrees Celsius. The laboratory will nacasitare; <br /> document and report the temperature of the sample container upon arrival at the laboratory., <br /> The analytical laboratory places a total of 2 ml of nitric acid•in some of the I liter bottles to <br /> reduce the pH to below 2 On an annual basis an extra preserved bottle will be filled with <br /> groundwater-and-the pH measured in the bottle.- It is"assumed that the PH will be-below 2: If it <br /> is not the field technician will add nitric acid in measured amounts until the pH is below 2_ This <br /> added quantity of acid will be placed in all the preserved bottlesAuring the following monitoring <br /> rounds until it is checked again the foffowing-yrar_--Sample..pH•-will. be.confirmed:at.the•.: <br /> laboratory and recorded. Deviations will be documented and reported by the laboratory, <br /> Samples;to be submitted for metals analysis-will. be filtered in the field- Filtering-will be <br /> performed using an in .line ;fiber mechanism which uses the-pumpingProcess-of_the-dedic aced <br /> pump to draw water through the 4 micron filter- A new filter will be used at each well. The new, <br /> filters will have a minimum of one filter volume of groundwater pressmized through them to <br /> reduce adsorption effects. The actual filtered-sample-will not be col ected-untH aminimurn of <br /> two filter volumes ofground has been passed through the filter. For wells without <br /> dedicated Pumps, the samples arc transferred from the bailer,through a.filter apparatus, into the <br /> appropriate sample container. The filter apparatus consists of a a pie <br /> Pr=urc PSP= and a filter cartridge- Water from the bailer is placed in the pressure vessel and <br /> enough air pressure(via the hand )is applied to force water through the filr_,er cartridge into <br /> the sample bottles_ Thep vessel is washed in Alconox, steam cleaned, and rinsed'with <br /> deicnized water between wells_ A new filter cartridge is used at each well_ <br /> ple$ will. be labeled with a unique sample identification number, project identification <br /> number, sample location, and date and time sampled. Samples will be transported to the contract <br /> labostory under strict chain-of-custodyprocedures- <br /> 23-483$4 9-F01%2310RM A-9 July 14,2Q40 <br /> 2000 AfGi(ilc fila.tv_ <br />