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purged according to the protocol presented in Figure A-1. In most moni- <br /> toring wells, the amount of water purged before sampling was equal to or <br /> greater than four casing volumes. Some monitoring wells were evacuated <br /> to dryness after the removal of less than four casing volumes. These low- <br /> yield monitoring wells were allowed to recharge for up to 24 hours. Samp- <br /> les were collected as soon as the monitoring wells had recharged to a <br /> level sufficient for sample collection. If insufficient water had recharged <br /> after 24 hours, the monitoring well was recorded as dry for the sampling <br /> event. <br /> Field measurements were recorded in a water-resistant field logbook. Fig- <br /> ure A-2 shows an example of the Water Sample Field Data Sheet on <br /> which field data were recorded. Field data sheets were reviewed by the <br /> sampling coordinator after the sampling event was completed. <br /> The pH, specific conductance, and temperature meter were calibrated <br /> each day before beginning field activities. The calibration was checked <br /> once each day to verify meter performance. Field meter calibrations were <br /> recorded on a Field Data Sheet (see Figure A-2). <br /> Well Sampling <br /> Teflon bailer or bladder pump was the only equipment acceptable for <br /> well sampling. When samples for volatile organic analysis were being col- <br /> lected with a bladder pump, the pump flow was regulated to approximately <br /> 100 milliliters per minute to minimize pump effluent turbulence and aera- <br /> tion. Glass bottles of at least 40 milliliters volume and fitted with Teflon- <br /> lined septa were used in sampling for volatile organics. These bottles were <br /> filled completely to prevent air from remaining in the bottle. A positive <br /> meniscus formed when the bottle was completely full. A convex Teflon <br /> septum was placed over the positive meniscus to eliminate air. After the <br /> bottle was capped, it was inverted and tapped to verify that it contained no <br /> air bubbles. The sample containers for other parameters were filled, fil- <br /> tered as required, and capped. <br /> To determine dissolved concentrations of metals, appropriate field filtration <br /> techniques were used. When a Teflon bailer was used, the sample was <br /> filtered by emptying the contents of the bailer into a pressure transfer ves- <br /> sel. A disposable 0.45-micron acrylic copolymer filter was threaded onto <br /> the transfer vessel at the discharge point and the vessel was sealed. <br /> Pressure was applied to the vessel with a hand pump and the filtrate was <br /> pj9\939\9390111 c A-4 Rev. 0 September 9, 1992 <br />