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110 2nd Avenue South,#D7,Pacheco CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925 798-1622 <br /> h //www mcc belLcom E-mail mainmccarMbell com <br /> Advanced GeoEnvironrnental,Inc Client Project ID Waterloo FF-Effluent Date Sampled 05/20/03 <br /> 837 Shaw Road Date Received 05/21/03 <br /> Client Contact Bill Little Date Extracted 05/21/03 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 05/23/03 <br /> Senuvolatiles Organics by GUMS(625 Basic Target List)" <br /> Extraction Method SW 3535A Analytical Method SWE27017 Work Order D305330 <br /> Lab ID 0305330-OOIB <br />' Client ID Effluent <br /> Matrix Water <br /> Compound I Concentration* rDFR Ling Compound Concentration* DF L` „rns a <br />' Acenaphthene ND 1 Acenaphthylene ND 10 10 <br /> Anthracene ND 10 Benzidine ND 10 5 <br /> Benz(a)anthracene ND 10 Benzo(b)fluoranthene ND 10 10 <br /> Benzo(k)Eluoranthene ND 10 Benzo(g,h,i)perylene ND 10 5 <br /> Benzo(a)pyrene ND 10 Bis(2-chloroethoxy)Methane ND1 0 5 <br /> Bis(2-chloroethyl)Ether ND 1 0 1 Bis(2-chloroisopropyl)Ether ND 1 0 2 <br /> Bis(2-ethylhexyl)Phthalate ND 1 0 5 4-Bromophenyl Phenyl Ether ND 1 0 5 <br />' Butylbenzyl Phthalate ND 1 0 10 4-Chloro-3-methylphen6 ND 10 1 <br /> 2-Chloronaphthalene ND 10 10 2-Chlorophenol ND 10 5 <br /> 4-Chlorophenyl Phenyi Ether ND 1 0 5 Chrysene ND 10 10 <br />' Dibenzo(a,h)anthracene ND 1 0 10 Di-n-butyl Phthalate ND 10 10 <br /> 1,2-Dichlorobenzene ND 1 0 2 1,3-Dichlorobenzene ND 10 1 <br /> 1,4-Dichlorobenzene ND 10 1 3,3-Dichlorobenzidme ND 10 5 <br />' • 2 4-Dichlorophenol ND 1 0 5 Diethyl Phthalate ND 1 0 2 <br /> 2,4-Dimethylphenol ND 1 0 2 Dimethyl Phthalate ND 10 2 <br /> 4,6-Dmitro-2-methylphenol ND 10 5 2,4-Dmitrophenol ND 10 5 <br /> 2 4-13iniimloluene ND 1 0 5 2 6-Dinitrotoluene ND 1 0 5 <br /> 1 Di-n-octyl Phthalate ND 1 0 10 1,2-Diphenyihydrazine ND 10 1 <br /> Fluoranthene ND 10 1 Fluorene ND 10 10 <br /> Hexachlarobenzene ND 10 1 Hexachlorobutadtene IIID 10 1 <br />' Hexachlorocyclopentadiene ND 10 5 Hexachloroethane ND 10 1 <br /> Indeno(1,2,3-cd)pyrene ND 1 0 10 Isophorone ND 1 0 1 <br /> Naphthalene ND 10 1 Nitrobenzene ND 10 1 1 <br /> 2-Nitrophenol ND 10 10 4-Nitrophenol ND 10 l0 <br /> N-Nitrosodimethylamine ND 10 5 N-Nitrosodiphenylamme ND 10 1 <br /> N-Nitrosodi-n-propylamine ND 1 0 5 Pentachlorophenol ND 10 5 <br /> Phenanthrene ND 10 5 Phenol ND 10 1 <br />' Pyrene ND 10 10 1,2,4-Tnchlorobenzene ND 10 5 <br /> 2,4,6-Trichlorophenol ND 10 1 10 <br /> Surrogate Recoveries(%) <br /> %SS 623 %S$ 786 <br /> %SS 656 %SS 746 <br /> %SS 721 %SS 561 <br />' Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in jig/L,soilisludge/solid samples in mg/kg, wipe samples in Ag/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peals <br />' h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than--2 vol %sediment,,/)sample diluted due to high <br /> organic content <br /> ' DHS Certification No 1644 Angela Rydeltus,Lab Manager <br />