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110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h Jlwww mccarripbell cam E-mail nurin@tnecarripbell com <br /> Advanced GeoEnvironmental, Inc Client Project ID Waterloo FF-Effluent Date Sampled 05/20/03 <br /> $37 Shaw Road Date Received 05/21/03 <br /> Client Contact Bill Little Date Extracted 05/21/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 05/21/03 <br /> LUFT 5 Metals+Copper* <br /> Extraction method E2007/E2009 Analytical methods 13200 7/13200 9 Work Order 0305330 <br />' Lab ID Client ID Matrix Extraction Cadmium Chromium Copper Lead Nickel Zinc DF %SS <br /> 001C Effluent W TTLC ND ND ND ND ND ND 1 106 <br /> -.F1 <br /> Reporting Limit for DF=1, py TTLC 0 020 101+001 0 005 005 1 005 mg/L <br /> ND means not detected at or <br /> above the reporting limit S TTLC NA NANA NA NA NA NA <br /> " water/liquid/oil samples are reported in mg/L,soil/sludge/solid/product samples in mg/kg,wipes in}rg/wipe and all TCLP/STLC/DISTLC/SPLP <br />' extracts in mg/L <br /> #means surrogate recovery outside of acceptance range due to matrix interference,ND means not detected above the reporting limit,N/A means not <br /> applicable to this sample or instrument <br /> Analytical Methods EPA 6010C/200 7 for all elements except 200 9(water/liquid-Sb,As,Pb,Se,TI),245 1 (Hg),7010 <br /> (sludge/soil/solid/oil/product/wipes-As,Sc,TI),7471B(Hg) <br /> i)liquid sample that contains greater than--2 vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br />' significantly effect reported metal concentrations,1)reporting limit raised due to insufficient sample amount,y)estimated values due to low surrogate <br /> recovery,z reporting limit raised due to matrix interference <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />