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A8L1471 Ekiiiiiiiiiiiiili General: Heavy Metals ASSOCIATES BSK Associates Laboratory Fresno Metals Quality Control Report Spike Source %REC RPD Date Analyte Result RL Units Level Result %REC Limits RPID Limit Analyzed Qual EPA 6020-Quality Control Batch:A818732 Prepared: 12/15/2018 Prep Method:EPA 3010A for TCLP(EPA 1311) Analyst: MAS Blank Spike Dup(A818732-BSD1) Nickel,TCLP 8.0 0.40 mg/L 8.0 ND 100 75-125 1 20 12/17/18 Selenium,TCLP 7.6 0.080 mg/L 8.0 ND 95 75-125 4 20 12/17/18 Silver,TCLP 3.7 0.40 mg/L 4.0 ND 93 75-125 1 20 12/17/18 Thallium,TCLP 7.6 0.50 mg/L 8.0 ND 95 75-125 0 20 12/17/18 Vanadium,TCLP 8.3 0.40 mg/L 8.0 ND 104 75-125 0 20 12/17/18 Zinc,TCLP 7.4 2.0 mg/L 8.0 ND 93 75-125 0 20 12/17/18 Duplicate(A818732-DUP1),Source:A81-1471-01 Antimony,TCLP ND 0.50 mg/L ND 20 12/17/18 Arsenic,TCLP ND 0.080 mg/L ND 20 12/17/18 Barium,TCLP 2.0 0.20 mg/L 2.2 9 20 12/17/18 Beryllium,TCLP ND 0.050 mg/L ND 20 12/17/18 Cadmium,TCLP ND 0.050 mg/L ND 20 12/17/18 Chromium,TCLP ND 0.40 mg/L ND 20 12/17/18 Cobalt,TCLP ND 0.40 mg/L ND 20 12/17/18 Copper,TCLP ND 0.20 mg/L ND 20 12/17/18 Lead,TCLP ND 0.20 mg/L ND 20 12/17/18 Molybdenum,TCLP ND 0.40 mg/L ND 20 12/17/18 Nickel,TCLP ND 0.40 mg/L ND 20 12/17/18 Selenium,TCLP ND 0.080 mg/L ND 20 12/17/18 Silver,TCLP ND 0.40 mg/L ND 20 12/17/18 Thallium,TCLP ND 0.50 mg/L ND 20 12/17/18 Vanadium,TCLP ND 0.40 mg/L ND 20 12/17/18 Zinc,TCLP ND 2.0 mg/L ND 20 12/17/18 Matrix Spike(A818732-MS1),Source:A81-1471-01 Antimony,TCLP 8.2 0.50 mg/L 8.0 ND 102 75-125 12/17/18 Arsenic,TCLP 8.0 0.080 mg/L 8.0 ND 100 75-125 12/17/18 Barium,TCLP 9.6 0.20 mg/L 8.0 2.2 93 75-125 12/17/18 Beryllium,TCLP 7.8 0.050 mg/L 8.0 ND 98 75-125 12/17/18 Cadmium,TCLP 7.7 0.050 mg/L 8.0 ND 96 75-125 12/17/18 Chromium,TCLP 8.2 0.40 mg/L 8.0 ND 103 75-125 12/17/18 Cobalt,TCLP 8.2 0.40 mg/L 8.0 ND 102 75-125 12/17/18 Copper,TCLP 7.9 0.20 mg/L 8.0 ND 99 75-125 12/17/18 Lead,TCLP 7.9 0.20 mg/L 8.0 ND 98 75-125 12/17/18 Molybdenum,TCLP 8.7 0.40 mg/L 8.0 ND 109 75-125 12/17/18 Nickel,TCLP 8.2 0.40 mg/L 8.0 ND 102 75-125 12/17/18 Selenium,TCLP 7.5 0.080 mg/L 8.0 ND 93 75-125 12/17/18 Silver,TCLP 3.8 0.40 mg/L 4.0 ND 96 75-125 12/17/18 Thallium,TCLP 7.8 0.50 mg/L 8.0 ND 98 75-125 12/17/18 Vanadium,TCLP 8.5 0.40 mg/L 8.0 ND 106 75-125 12/17/18 Zinc,TCLP 7.7 2.0 mg/L 8.0 ND 96 75-125 12/17/18 Matrix Spike Dup(A818732-MSD1),Source:A81-1471-01 Antimony,TCLP 8.0 0.50 mg/L 8.0 ND 100 75-125 2 20 12/17/18 Arsenic,TCLP 7.8 0.080 mg/L 8.0 ND 98 75-125 3 20 12/17/18 The results in this report apply to the samples analyzed in A811471 FINAL 12272018 1717 accordance with the chain of custody document. This analytical report must be reproduced in its entirety. www.BSKAssociates.com Page 8 of 18